Low cost apparatus for rapid boiling point determination of small air sensitive samples under inert atmosphere

摘要

Highlights ? Rapid boiling point determination (15min). ? Small sample volumes of 0.05–0.2ml. ? Working under inert atmosphere with standard Schlenk technique. ? Simple and low cost apparatus. Abstract The boiling point is a characteristic property of substances and mixtures. We have developed a new low cost apparatus which uses standard Schlenk technique for measuring the boiling point of small samples (0.2ml) under inert a