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Rheological properties of contemporary nanohybrid dental resin composites: The influence of preheating

机译:当代纳米牙科树脂复合材料的流变性质:预热的影响

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摘要

Preheating of dental composites enhances their flowability and can improve marginal adaptation and decrease voids leading to more successful restorations. The aim of this research is to study the influence of preheating temperature on the rheological properties of four contemporary nanohybrid dental resin composites. The rheological measurements on the four preheated nanohybrid resin-based composites [Herculite Ultra (Kerr), Tetric EvoCeram (Ivoclar Vivadent), Filtek Supreme Ultra (3 M) and Grandio (Voco)] were conducted utilizing a parallel-plate shear rheometer. The composites were placed on the lower plate, and the upper plate was lowered until it gently touched the surface of the sample at a gap distance of 0.5 mm. Measurements were obtained at three different temperatures 25, 37 and 60 degrees C. The shear rate varied linearly in ramp mode from 0.1 to 10 s(-1). All dental resin composites tested in this research showed a significant reduction in shear viscosity with increasing temperature. Additionally, all dental resin composites were pseudoplastic, indicating a disproportionate reduction in complex viscosity (eta*) with enhancing frequency (shear rate; shear-thinning effects). There is a variation in shear modulus of elasticity (G') between the four contemporary nanohybrid dental resin composites at low shear rates. Preheating the composite material resulted in enhanced flow and greater adaptability, as evident by decreasing G' values with increasing shear rate which did not occur with samples that were not preheated. The results demonstrated that regardless of the resin composite material, it was found that preheating the nanohybrid dental composites considerably improves their flowability and can improve clinical placement and adaptation. Finally, the obtained results could be employed as a guideline for material behavior to form the desired consistency or compare commercially available preheating devices.
机译:牙科复合材料的预热增强了它们的流动性,可以改善边缘适应并降低导致更成功的修复的空隙。本研究的目的是研究预热温度对四种现代纳米牙科牙科树脂复合材料的流变性能的影响。使用平行板剪切流变仪进行四种预热的纳米组合材料[母细胞超(kerr),Tetric evocraram(Ivoclar VieveraM),Filtek至尊超超(3 m)和Grandio(Voco)的流变学测量。将复合材料置于下板上,下板降低直至其在0.5mm的间隙距离下轻轻地触摸样品的表面。在三个不同温度25,37和60℃下获得测量。剪切速率在0.1至10 s(-1)中以斜坡模式线性变化。在该研究中测试的所有牙科树脂复合材料显示出剪切粘度的显着降低,温度升高。另外,所有牙科树脂复合材料都是假塑性的,表明复合粘度(ETA *)的减少,增强频率(剪切速率;剪切稀疏效果)。在低剪切速率下,四种现代纳米牙科树脂复合材料之间存在剪切弹性(G')的剪切弹性模量。预热复合材料导致流动增强和更大的适应性,通过降低G'值随着未预热的样品而没有发生的剪切速率而显然。结果表明,无论树脂复合材料如何,发现预热纳米牙科复合材料大大提高了流动性,可以改善临床放置和适应。最后,可以使用所得结果作为材料行为的指导,以形成所需的一致性或比较市售的预热装置。

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