Molecular characteristics of polymerized surfactants: influence of introduced crosslinking agent and monomer concentration

Senchukova Anna S; Mikhailova Mariya E; Gubarev Alexander S; Lezov Alexey A; Lebedeva Elena V; Makarov Ivan A; Zorin Ivan M; Tsvetkov Nikolay V

摘要

Abstract > Polymerizable surfactants are currently attracting considerable interest due to their promising applications in various fields of science and engineering. The present work is devoted to studies of crosslinked poly( N ‐acryloyl‐11‐aminoundecanoic acid) and sodium poly( N ‐acryloyl‐11‐aminoundecanoate) that were synthesized in reaction mixtures of various compositions (i.e. with different amounts of a crosslinking agent and monomer concentrations). The products were studied by viscometry, dynamic light scattering, sedimentation velocity ultracentrifugation, flow birefringence as well as equilibrium and non‐equilibrium electric birefringence. It was established that both intramolecular and intermolecular crosslinks are formed in the polymerization process. Molecular optical methods and electro‐optical methods were used to determine the sizes of macromolecules with intramolecular crosslinks and the structures containing intermolecular crosslinks that were prepared at various concentrations of the monomer and the crosslinking agent. It was demonstrated that a simultaneous decrease in the amount of the crosslinking agent and decrease in the initial monomer concentration during the synthesis resulted in a reduction in the number of intramolecular crosslinks and molecular masses of the synthesized crosslinked macromolecules. ? 2019 Society of Chemical Industry </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 由于其在各种科学和工程领域的希望应用，可聚合表面活性剂目前吸引了相当大的利益。本作本作研究了交联多（ n </ i> - 丙烯酰基-11-氨基磺酸）和钠聚（ n </ i> - 在各种组合物的反应混合物中合成的 - 丙烯酰基-11-氨基烷烃（即用不同量的交联剂和单体浓度）。通过粘度，动态光散射，沉降速度超速离心，流动双折射以及平衡和非平衡电动双折射来研究该产品。建立了分子内和分子间交联中的聚合过程中的形成。分子光学方法和电光方法用于测定具有分子内交联的大分子大小和含有在各种浓度的单体和交联剂的分子间交联的结构。证明其在合成期间交联剂量的同时减少和初始单体浓度的降低导致合成交联大分子的分子内交联和分子量的数量降低。还2019年化学工业学会 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29710/'>《Polymer international》</a> <b style="margin: 0 2px;">|</b><span>2020年第1期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Senchukova Anna S&option=202" target="_blank" rel="nofollow">Senchukova Anna S;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mikhailova Mariya E&option=202" target="_blank" rel="nofollow">Mikhailova Mariya E;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gubarev Alexander S&option=202" target="_blank" rel="nofollow">Gubarev Alexander S;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lezov Alexey A&option=202" target="_blank" rel="nofollow">Lezov Alexey A;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lebedeva Elena V&option=202" target="_blank" rel="nofollow">Lebedeva Elena V;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Makarov Ivan A&option=202" target="_blank" rel="nofollow">Makarov Ivan A;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zorin Ivan M&option=202" target="_blank" rel="nofollow">Zorin Ivan M;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tsvetkov Nikolay V&option=202" target="_blank" rel="nofollow">Tsvetkov Nikolay V;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Molecular Biophysics and Physics of PolymersSt Petersburg State UniversitySt Petersburg Russia;</p> <p>Department of Molecular Biophysics and Physics of PolymersSt Petersburg State UniversitySt Petersburg Russia;</p> <p>Department of Molecular Biophysics and Physics of PolymersSt Petersburg State UniversitySt Petersburg Russia;</p> <p>Department of Molecular Biophysics and Physics of PolymersSt Petersburg State UniversitySt Petersburg Russia;</p> <p>Department of Molecular Biophysics and Physics of PolymersSt Petersburg State UniversitySt Petersburg Russia;</p> <p>Department of Macromolecular Chemistry Institute of ChemistrySt Petersburg State UniversitySt Petersburg Russia;</p> <p>Department of Macromolecular Chemistry Institute of ChemistrySt Petersburg State UniversitySt Petersburg Russia;</p> <p>Department of Molecular Biophysics and Physics of PolymersSt Petersburg State UniversitySt Petersburg Russia;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=crosslinked polymer&option=203" rel="nofollow">crosslinked polymer;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=macromolecule conformation&option=203" rel="nofollow">macromolecule conformation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hydrodynamics&option=203" rel="nofollow">hydrodynamics;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=optical characteristics&option=203" rel="nofollow">optical characteristics;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electro‐optical characteristics&option=203" rel="nofollow">electro‐optical characteristics;</a> </p> <div class="translation"> 机译：交联聚合物;大分子构象;流体动力学;光学特性;电光特性; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024575635.html">Molecular characteristics of polymerized surfactants: influence of introduced crosslinking agent and monomer concentration</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Senchukova Anna S&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Senchukova Anna S,</a> <a 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=马利成&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,马利成</a> <span> <a href="/journal-cn-56724/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 油田化学 </a> </span> <span> . 2003</span><span>,第4期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-18977_thesis/020222128966.html">化学聚合条件对聚合物叠层铝电解电容器电性能的影响Ⅰ.单体浓度和氧化剂的影响</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . </a> <span> <a href="/conference-cn-18977/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国电子学会第十五届电子元件学术年会 </a> <span> <span> . 2008</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020311518874.html">染料与可聚合液晶单体浓度对胆甾相液晶激光的影响规律研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王仲阳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王仲阳</a> <span> . 2014</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120101777197.html">预交联剂浓度对压裂堵剂成胶性能影响的测试方法</a> <b>[P]</b> . <span> 中国专利： CN103048237A </span> <span> . 2013-04-17</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120101777766.html">用于测试二次交联剂浓度对压裂堵剂成胶性能影响的方法</a> <b>[P]</b> . <span> 中国专利： CN103048435A </span> <span> . 2013-04-17</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130472403464.html">Aqueous coating composition comprising a dispersion of polymerized unsaturated monomers, a nonionic surfactant and crosslinking agent</a> <b>[P]</b> . <span> 外国专利：  US4524173A </span> <span> . 1985-06-18</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包含聚合的不饱和单体，非离子表面活性剂和交联剂的分散体的水性涂料组合物 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130418663980.html">Aqueous polymerization of fluorinated monomers using a polymerization agent comprising a salt or surfactant fluoropolyether acids or salts and high molecular weight fluoropolyether acid</a> <b>[P]</b> . <span> 外国专利：  JP5470044B2 </span> <span> . 2014-04-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用包含盐或表面活性剂氟聚醚酸或盐和高分子量氟聚醚酸的聚合剂对氟化单体进行水聚合 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130425603590.html">Aqueous polymerization of fluorinated monomer using polymerization agent comprising high molecular weight fluoropolyether acid or salt and fluoropolyether acid or salt surfactant</a> <b>[P]</b> . <span> 外国专利：  US7932333B2 </span> <span> . 2011-04-26</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用包含高分子量氟聚醚酸或盐和氟聚醚酸或盐表面活性剂的聚合剂进行氟化单体的水聚合 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704024575635','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img 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