Highly Dispersed ZnSe Nanoparticles Embedded in N‐Doped Porous Carbon Matrix as an Anode for Potassium Ion Batteries

Hu Yi; Lu Tiantian; Zhang Ya; Sun Yongwen; Liu Jinlong; Wei Denghu; Ju Zhicheng; Zhuang Quanchao

摘要

Abstract > Advanced nanostructured functional materials obtained from the precursors of metal–organic frameworks show several unique advantages, including plentiful porous structures and large specific surface areas. Based on this, designed and constructed are highly dispersed ZnSe nanoparticles anchored in a N‐doped porous carbon rhombic dodecahedron (ZnSe@NDPC) by a sequential high‐temperature pyrolysis and selenization method. The specific synthesis process involves a two‐step heat treatment of the template‐engaged reaction between zinc‐based zeolitic imidazolate framework (ZIF‐8) and selenium power. By optimizing the calcination temperature, the as‐synthesized ZnSe@NDPC‐700 as an advanced anode of potassium ion batteries demonstrates the best electrochemical performance, including a high capacity (262.8 mA h g ?1 over 200 cycles at 100 mA g ?1 ) and a good rate capability (109.4 mA h g ?1 at 2000 mA g ?1 and 52.8 mA h g ?1 at 5000 mA g ?1 ). Moreover, the capacitance and diffusion mechanisms are also investigated by the qualitative and quantitate analysis, finally accounting for the superior K storage. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 从金属 - 有机框架的前体获得的先进的纳米结构官能材料显示出几种独特的优点，包括丰富的多孔结构和大的比表面积。基于此，通过顺序高温热解和硒化方法，设计和构造的高度分散在N掺杂多孔碳菱形十二烷（ZnSe @ NDPC）中的高度分散的ZnSe纳米颗粒。特定的合成方法涉及锌基沸石咪唑酯骨架（ZIF-8）和硒功率之间的模板接合反应的两步热处理。通过优化煅烧温度，作为钾离子电池的先进阳极的AS合成的ZnSe @ NDPC-700证明了最佳的电化学性能，包括高容量（262.8 ma H g ？1 </ sup> 100 mA g超过200周期？1 </ sup> ）和良好的速率能力（109.4 ma H g ？1 </ sup> 在2000 ma g ？1 </ sup> 和52.8 ma h g ？1 </ sup> 在5000 ma g ？1 </ sup> ）。此外，还通过定性和定量分析研究了电容和扩散机制，最后占高级K储存。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-28901/'>《Particle & Particle Systems Characterization: Measurement and Description of Particle Properties and Behavior in Powders and Other Disperse Systems》</a> <b style="margin: 0 2px;">|</b><span>2019年第10期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hu Yi&option=202" target="_blank" rel="nofollow">Hu Yi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lu Tiantian&option=202" target="_blank" rel="nofollow">Lu Tiantian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Ya&option=202" target="_blank" rel="nofollow">Zhang Ya;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sun Yongwen&option=202" target="_blank" rel="nofollow">Sun Yongwen;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Jinlong&option=202" target="_blank" rel="nofollow">Liu Jinlong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wei Denghu&option=202" target="_blank" rel="nofollow">Wei Denghu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ju Zhicheng&option=202" target="_blank" rel="nofollow">Ju Zhicheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhuang Quanchao&option=202" target="_blank" rel="nofollow">Zhuang Quanchao;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>The Jiangsu Province Engineering Laboratory of High Efficient Energy Storage Technology and EquipmentsChina University of Mining and TechnologyXuzhou 221116 P. R. China;</p> <p>The Jiangsu Province Engineering Laboratory of High Efficient Energy Storage Technology and EquipmentsChina University of Mining and TechnologyXuzhou 221116 P. R. China;</p> <p>The Jiangsu Province Engineering Laboratory of High Efficient Energy Storage Technology and EquipmentsChina University of Mining and TechnologyXuzhou 221116 P. R. China;</p> <p>The Jiangsu Province Engineering Laboratory of High Efficient Energy Storage Technology and EquipmentsChina University of Mining and TechnologyXuzhou 221116 P. R. China;</p> <p>The Jiangsu Province Engineering Laboratory of High Efficient Energy Storage Technology and EquipmentsChina University of Mining and TechnologyXuzhou 221116 P. R. China;</p> <p>School of Materials Science and EngineeringLiaocheng UniversityLiaocheng Shandong 252059 P. R. China;</p> <p>The Jiangsu Province Engineering Laboratory of High Efficient Energy Storage Technology and EquipmentsChina University of Mining and TechnologyXuzhou 221116 P. R. China;</p> <p>The Jiangsu Province Engineering Laboratory of High Efficient Energy Storage Technology and EquipmentsChina University of Mining and TechnologyXuzhou 221116 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=N‐doped porous carbon&option=203" rel="nofollow">N‐doped porous carbon;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=potassium‐ion batteries&option=203" rel="nofollow">potassium‐ion batteries;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZIF‐8&option=203" rel="nofollow">ZIF‐8;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZnSe&option=203" rel="nofollow">ZnSe;</a> </p> <div class="translation"> 机译：n掺杂多孔碳;钾离子电池;ZIF-8;ZnSe; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul 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href="/academic-journal-cn_chinese-journal-inorganic-chemistry_thesis/0201277591606.html">熔盐锌热法制备三维多孔碳用于高性能钾离子电池负极材料</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=马凯&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 马凯</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=林宁&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,林宁</a> <span> <a href="/journal-cn-15070/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 无机化学学报 </a> </span> <span> . 2020</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chemistry-bioengineering_thesis/0201278408074.html">模板法制备多孔碳修饰微生物燃料电池阳极的研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=邢晓晔&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 邢晓晔</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘中良&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘中良</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈稳稳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈稳稳</a> <span> <a href="/journal-cn-9126/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 化学与生物工程 </a> </span> <span> . 2020</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-8345_thesis/020222122672.html">有机太阳电池阳极Pt纳米颗粒修饰及其性能研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liru Li&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . Liru Li</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李利如&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李利如</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Zhang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Yang Zhang</a> <span> <a href="/conference-cn-8345/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十七届全国化合物半导体材料微波器件和光电器件学术会议 </a> <span> <span> . 2012</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020315622679.html">多孔碳基材料用于高性能钾离子电池负极的研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张申魁&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 张申魁</a> <span> . 2020</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120112995043.html">一种应用于钠离子电池的N掺杂多孔碳负载ZnSe电极材料</a> <b>[P]</b> . <span> 中国专利： CN113023686A </span> <span> . 2021-06-25</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061204480096.html">一种用于高性能钾硫电池正极N掺杂Co纳米团簇/N掺杂多孔碳/S复合材料的制备方法</a> <b>[P]</b> . <span> 中国专利： CN111180700B </span> <span> . 2021.06.22</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130426775774.html">Producing an electrically conductive porous carbon material useful as a battery anode material comprises incorporating silicon and/or tin nanoparticles into a polymer matrix and carbonizing the product</a> <b>[P]</b> . <span> 外国专利：  DE102009033251A1 </span> <span> . 2010-09-23</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：制备用作电池负极材料的导电多孔碳材料包括将硅和/或锡纳米颗粒掺入聚合物基体中并使产品碳化 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130403328745.html">- Spider network structure composition of N-doped carbon nanofibers containing MnCoOx nanoparticles the preparation method and application to anode material for secondary battery</a> <b>[P]</b> . <span> 外国专利：  KR20190011362A </span> <span> . 2019-02-07</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：-含MnCoOx纳米粒子的N掺杂碳纳米纤维的蜘蛛网状结构组成，制备方法及其在二次电池负极材料中的应用 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130403148206.html">- Spider network structure composition of N-doped carbon nanofibers containing MnCoOx nanoparticles the preparation method and application to anode material for secondary battery</a> <b>[P]</b> . <span> 外国专利：  KR101997968B1 </span> <span> . 2019-07-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：-含MnCoOx纳米粒子的N掺杂碳纳米纤维的蜘蛛网状结构组成，制备方法及其在二次电池负极材料中的应用 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704024384475','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="关闭" onclick="$('.journalsub-pop-up').hide()"> <p class="pardon">抱歉，该期刊暂不可订阅，敬请期待！</p> <p 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