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Low cycle fatigue performance of Ni-based superalloy coated with complex thermal barrier coating

机译:基于Ni的高温合金涂覆复合热阻挡涂层的低循环疲劳性能

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Thermal barrier coatings (TBCs) are widely applied to protect high-temperature components against high temperatures in harsh environments. Nineteen cylindrical specimens of Inconel 713LC were manufactured using the investment castings technique, and 10 specimens were subsequently coated with a novel complex thermal barrier coating (TBC) system. The TBC system comprises a metallic CoNiCrAlY bond coat (BC) and a complex ceramic top coat (TC). The TC is a mixture of a near eutectic nanocrystalline ceramic made of zirconia (ZrO2), alumina (Al2O3), silica (SiO2) and conventional yttria stabilized zirconia (YSZ) ceramic in the ratio of 50/50 in wt%. Low cycle fatigue (LCF) tests were carried out in a symmetrical push-pull cycle under strain control at 900 degrees C. Cyclic hardening/softening curves, cyclic stress-strain curves and fatigue life curves of the TBC-coated and uncoated material were assessed. Fatigue life curves in total strain representation showed transient behaviour. Fracture surfaces and polished sections parallel to the loading axis of the TBC-coated and uncoated specimens prior and after cyclic loading were observed by means of scanning electron microscopy (SEM) to study the degradation mechanisms during high-temperature LCF. TBC delamination was observed at the TC/BC interface, and rafting of precipitates occurred after high-temperature exposure. The microstructural investigations further the discussion of the differences in the stress-strain response and the fatigue life of the TBC-coated and uncoated superalloy.
机译:热阻涂层(TBC)广泛应用于保护高温分量免受恶劣环境中的高温。 Inconel 713LC的19个圆柱形标本使用投资铸件技术制造,随后用新型复杂的热阻挡涂层(TBC)系统涂覆10个样本。 TBC系统包括金属聚焦粘结涂层(BC)和复杂的陶瓷顶部涂层(TC)。 TC是由氧化锆(ZrO2),氧化铝(Al 2 O 3),二氧化硅(SiO 2)和常规氧化钇稳定的氧化锆(YSZ)陶瓷制成的近共晶纳米晶陶瓷的混合物,其比例为50/50的WT%。低循环疲劳(LCF)测试在900摄氏度的应变控制下在对称的推挽循环中进行。评估循环硬化/软化曲线,循环硬化/软化曲线,循环应力 - 应变曲线和TBC涂层和未涂覆材料的疲劳寿命曲线。总应变表示中的疲劳寿命曲线显示出瞬态行为。通过扫描电子显微镜(SEM)观察到与TBC涂覆和未涂覆的样品的加载轴平行的断裂表面和抛光部分通过扫描电子显微镜(SEM)来研究高温LCF期间的降解机制。在TC / BC界面观察到TBC分层,高温暴露后发生沉淀物的漂流。微观结构研究进一步讨论了应力 - 应变反应的差异和TBC涂覆和未涂覆超合金的疲劳寿命。

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