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Simultaneous Anodic Adsorptive Stripping Voltammetric Determination of Luteolin and 3‐Hydroxyflavone in Biological Fluids Using Renewable Pencil Graphite Electrodes

机译：使用可再生铅笔石墨电极同时阳极阳极吸附剥离伏安法测定生物流体中的叶黄素和3-羟基硫酮

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Abstract > Simultaneous anodic adsorptive stripping voltammetry was applied for selective and sensitive electrochemical determination of the flavones luteolin (LU) and the basic flavone core 3‐hydroxyflavone (3HF) using a renewable pencil graphite electrode (PGE). The increased separation of the anodic peak potential of LU and 3HF on a PGE surface together with the increased sensitivity renders their simultaneous determination feasible by square wave anodic adsorptive stripping voltammetry (SWAASV). The electrochemical parameters such as surface concentration (Γ), electron transfer coefficient (α), and the standard rate constant (k <sub>s</sub> ) of both LU and 3HF at a PGE were calculated. For simultaneous detection of both compounds by synchronous change of the concentration of LU and 3HF, the detection limits were 1.34?nM and 5.15?nM, respectively. The proposed procedure was successfully applied for the simultaneous detection of LU and 3HF in human serum and urine samples with satisfactory results. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract type =“main”xml：lang =“en”> <标题类型=“main”>摘要</ title> >同时阳极吸附剥离伏安法应用于选择性和敏感的电化学测定黄酮叶英蛋白的选择性和敏感的电化学测定（Lu ）和使用可再生铅笔石墨电极（PGE）的基本黄酮核心3-羟基氟（3HF）。 Lu和3HF的阳极峰值电位的分离的增加与PGE表面的增加的敏感性使得其同时测定由方波阳极吸附剥离伏安法（SWAASV）可行。计算诸如表面浓度（γ），电子传递系数（α）的电化学参数，以及在PGA下的LU和3HF的标准速率常数（k <亚> s </ sub>）。通过通过Lu和3HF浓度的同步变化同时检测两种化合物，检测限为1.34Ω·Nm和5.15？nm。所提出的程序成功地应用于同时检测人血清和尿液样本的LU和3HF，结果令人满意。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2019年第6期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Temerk Yassien&option=202" target="_blank" rel="nofollow">Temerk Yassien;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ibrahim Hossieny&option=202" target="_blank" rel="nofollow">Ibrahim Hossieny;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Schuhmann Wolfgang&option=202" target="_blank" rel="nofollow">Schuhmann Wolfgang;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Chemistry DepartmentAssiut UniversityAssiut Egypt;</p> <p>Chemistry DepartmentAssiut UniversityAssiut Egypt;</p> <p>Analytical Chemistry – Center for Electrochemical Sciences (CES)Ruhr University Bochum D-44780 Bochum Germany;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=3-hydroxyflavone&option=203" rel="nofollow">3-hydroxyflavone;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=luteolin&option=203" rel="nofollow">luteolin;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=anodic stripping voltammetry&option=203" rel="nofollow">anodic stripping voltammetry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=biological fluids&option=203" rel="nofollow">biological fluids;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=pencil graphite electrode&option=203" rel="nofollow">pencil graphite electrode;</a> </p> <div class="translation"> 机译：3-羟基噻酮;叶黄素;阳极剥离伏安法;生物流体;铅笔石墨电极; 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