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Stable and Sensitive Amperometric Determination of Endocrine Disruptor Bisphenol A at Residual Metal Impurities Within SWCNT

机译：SWCNT内残留金属杂质在残留金属杂质中的稳定和敏感的水平测定稳定和敏感的水平测定

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Abstract > A simple and attentive method was attempted for the determination of endocrine disruptor molecule, Bisphenol A (BPA) using residual metal impurity act as a reactant present in as received SWCNT. The electrochemical behavior of BPA oxidation and its reaction mechanism was investigated by cyclic voltammetry using “as received SWCNT modified on glassy carbon electrode” (SWCNT/GCE) and the obtained results were compared with bare GCE. The SWCNT/GCE showed high electrocatalytic activity, sensitivity, stability and more importantly not much surface fouling compared with bare GCE. This is because of the formation of electroactive quinone and catechol as byproducts on SWCNT/GCE during electro‐oxidation of BPA. More interestingly, the electrochemically acid treated SWCNT/GCE not showed any characteristic oxidation and reduction peaks during electro‐oxidation of BPA which indicates that the presence of a residual metal impurity in SWCNT plays a vital role in electro‐oxidation of BPA. The amperometric detection of BPA oxidation on SWCNT/GCE showed excellent stability and good linear response from the wide range of concentration of 10–100?μM. The limit of detection and sensitivity of BPA electro‐oxidation on SWCNT/GCE is to be 7.3?μM (S/N=3) and 0.6494?μA/μM?cm 2 respectively. Finally, the fabricated sensor using SWCNT/GCE was successfully applied for the detection of BPA in plastic water bottles with excellent recovery range from 98–102?%. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</ title> >试图确定内分泌干扰分子，双酚A（BPA）的测定）使用残留的金属杂质作为所接收的SWCNT中存在的反应物。通过循环伏安法使用“如玻璃碳电极上修饰的接收的SWCNT”（SWCNT / GCE）的循环伏安法研究了BPA氧化及其反应机理的电化学行为，并将得到的结果与裸GCE进行了比较。与裸GCE相比，SWCNT / GCE显示出高电催化活性，敏感度，稳定性，更重要的是表面污垢。这是因为在BPA的电氧化过程中形成电活性醌和儿茶酚作为SWCNT / GCE的副产物。更有意义地，电化学酸处理的SWCNT / GCE未显示出BPA的电氧化过程中的任何特征氧化和还原峰，这表明SWCNT中残留金属杂质的存在在BPA的电氧化中起着至关重要的作用。在SWCNT / GCE上的BPA氧化的安培测定检测显示出优异的稳定性和良好的浓度为10-100Ωμm的线性响应。 SWCNT / GCE上BPA电氧化的检测和灵敏度的极限分别为7.3Ωμm（S / N = 3）和0.6494ΩΩΩ/μmαcm 2 </ sup>。最后，使用SWCNT / GCE的制造传感器被成功地应用于在塑料水瓶中检测BPA，其恢复的优异率为98-102倍。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2018年第3期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kanagavalli Pandiyaraj&option=202" target="_blank" rel="nofollow">Kanagavalli Pandiyaraj;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Senthil?Kumar Shanmugam&option=202" target="_blank" rel="nofollow">Senthil?Kumar Shanmugam;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Electrodics and Electrocatalysis DivisionCSIR-Central Electrochemical Research InstituteKaraikudi India;</p> <p>Electrodics and Electrocatalysis DivisionCSIR-Central Electrochemical Research InstituteKaraikudi India;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Residual metal impurity&option=203" rel="nofollow">Residual metal impurity;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=SWCNT&option=203" rel="nofollow">SWCNT;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bisphenol A&option=203" rel="nofollow">Bisphenol A;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Quinone&option=203" rel="nofollow">Quinone;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Catechol&option=203" rel="nofollow">Catechol;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Amperometric Sensor&option=203" rel="nofollow">Amperometric Sensor;</a> </p> <div class="translation"> 机译：残余金属杂质;SWCNT;双酚A;奎松;儿茶酚;安培传感器; </div> </li> </ul> </div> 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