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Multi-Step Cure Process for Void-Free Silicone Resin Encapsulant

机译:无空隙有机硅树脂密封剂的多步固化工艺

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摘要

In general, rapid cure reaction for LED encapsulant silicone resin causes serious defects in the cured resin product such as warpage, residual void, and decreasing wetablility. In order to remove residual voids in a silicone resin, multi-step cure processes were tested in the present investigation. Three kinds of multi-step cure processes were applied and residual voids were observed. Experimental observation showed that most of the voids were removed under 70℃ which is the minimum temperature for activating chemical cure reaction. In addition, degree of cure (DOC) and temperature distribution were predicted by using FEM analysis of heat transfer. It was concluded that cure temperature of the DOC smaller than 0.5~0.6 is an effective way to minimize the residual void and stress.
机译:通常,LED密封剂有机硅树脂的快速固化反应会在固化的树脂产品中造成严重的缺陷,例如翘曲,残余空隙和降低的可塑性。为了去除有机硅树脂中的残留空隙,在本研究中测试了多步固化工艺。应用了三种多步固化工艺,并观察到残留的空隙。实验观察表明,在激活化学固化反应的最低温度70℃以下,大部分空隙被去除。此外,通过使用传热的有限元分析来预测固化度(DOC)和温度分布。得出结论:DOC的固化温度小于0.5〜0.6是减少残余空隙和应力的有效途径。

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