Optimization and Evaluation of Applicability of HPLC for Validation of the Quality Index of Polyvitamin Pharmaceuticals

V. N. Filimonov; O. V. Zamuruev; L. N. Balyatinskaya

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Optimization and Evaluation of Applicability of HPLC for Validation of the Quality Index of Polyvitamin Pharmaceuticals

机译：HPLC适用性优化与评价，用于验证Polyvitamin Pharmaceuticals的质量指标

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Developed is a method of quantitative isolation and choise of optimal separation conditions of ester forms of lipid-solved vitamins E and A in conditions of HPLC. The method includes a procedure of mathematical design of experiment on the basis of Sheffe simplex-lattice plan {3, 3}. A possibility of using HPLC in combination with extraction procedures of sample preparation is shown for validation of the quality index of polyvitamin pharmaceuticals "PANGEKSAVIT", "DEKAMEVIT", and "TRIOVIT".

机译：开发的是一种定量分离和选择酯类脂质溶解维生素E的最佳分离条件的方法和HPLC条件。该方法包括基于Sheffe Simplex-leatice计划的实验的数学设计程序{3,3}。显示了使用HPLC与样品制备的提取程序组合的可能性显示用于验证Polyvitamin Pharmaceuticals“Paneksavit”，“DekameVit”和“Triovit”的质量指标。

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《Industrial Laboratory: Diagnostics of Materials》 |2001年第10期|共6页
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V. N. Filimonov; O. V. Zamuruev; L. N. Balyatinskaya;
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1. Optimization and Evaluation of Applicability of HPLC for Validation of the Quality Index of Polyvitamin Pharmaceuticals [J] . V. N. Filimonov, O. V. Zamuruev, L. N. Balyatinskaya Industrial Laboratory: Diagnostics of Materials . 2001,第10期

机译：高效液相色谱法用于验证维生素类药物质量指标的优化和评估
2. QUALITY BY DESIGN BASED OPTIMIZATION AND VALIDATION OF NEW RP-HPLC METHOD FOR SIMULTANEOUS ESTIMATION OF LEVOFLOXACIN HEMIHYDRATE AND AMBROXOL HCL IN BULK AND ITS PHARMACEUTICAL DOSAGE FORM [J] . Sumithra Sumithra Asian Journal of Pharmaceutical and Clinical Research . 2016,第suppla3期

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3. Chemometrically assisted optimization and validation of a new HPLC method for the determination of paliperidone in pharmaceuticals [J] . Sakine Atila Karaca, Duygu Yeniceli U?ur Journal of liquid chromatography and related technologies . 2018,第1a4期

机译：化学辅助优化和验证新型HPLC方法，用于测定药物中的Paliperidone
4. HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) INSTRUMENTATION CALIBRATION AND VALIDATION - CURRENT THEORIES AND PRACTICES IN THE PHARMACEUTICAL INDUSTRY [C] . KEN HOGLUND, NCSL NCSL Workshop and Symposium . 1998

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5. Part I. Evaluation of silver as a reductive amperometric detector electrode for HPLC and FIA. Part II. Evaluation of supercritical fluid extraction (SFE) as a sample preparation technique. Part III. Development and validation of HPLC methods using supercritical fluid extraction and reversed-phase HPLC with electrochemical detection (LCEC). [D] . Schneiderman, Martin Alan. 1990

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Optimization and Evaluation of Applicability of HPLC for Validation of the Quality Index of Polyvitamin Pharmaceuticals

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