A Low‐Sensitivity Nanocomposite of CL‐20 and TATB

Li Ping; Liu Kai; Ao Denggaowa; Liu Xun; Xu Haifeng; Duan Xiaohui; Pei Chonghua

摘要

Abstract >In order to improve the safety of 2,4,6,8,10,12‐hexanitro‐2,4,6,8,10,12‐hexaazaisowurtzitane (CL‐20) while preserving its high energy yield, a nanocomposite containing CL‐20 and 1,3,5‐triamino‐2,4,6‐trinitrobenzene (TATB) with a particular structure is prepared using an facile and fast antisolvent crystallization method. Using this approach, which takes advantage of strong antisolvent and temperature effects, a lamellar arrangement structure is created consisting of nanosheets containing CL‐20 and TATB, and further coated with dendritic nanometer‐scale TATB. XRD and Raman spectra indicate that CL‐20 in the resulting nanocomposite takes the form of α polymorph owing to the presence of ultrapure water. The HPLC results show that the TATB content of the nanocomposite is 20.2 wt%. When the surface coating of TATB is removed, 8 wt% TATB remains between the internal nanosheets. Due to the multiple desensitization effects of this structure, the nanocomposite has much lower sensitivity, roughly comparable to that of the insensitive explosive LLM‐105. Thermal analysis by thermogravimetry (TG) and differential scanning calorimeter indicates that the thermal decomposition activity of the nanocomposite is higher than those of raw materials, and in addition, its thermal stability is greater. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >，以提高2,4,6,8,10,12-12-己腈-2,4,6,8,10,12-六己唑尿丁烷（CL-20），同时保持其高能量产率，含有Cl-20和1,3,5-三氨基-2,4,6-三硝基苯的纳米复合材料（使用容易和快速的防溶剂结晶方法制备具有特定结构的TATB）。利用这种方法，利用强抗溶剂和温度效应，由含有Cl-20和TATB的纳米片组成的层状布置结构，并进一步涂有树突纳米级TATB。 XRD和拉曼光谱表明所得纳米复合材料中的Cl-20由于超纯水的存在而采用α多晶硅的形式。 HPLC结果表明，纳米复合材料的TATB含量为20.2wt％。当除去TATB的表面涂层时，内部纳米片之间的8wt％TATB仍然存在。由于这种结构的多脱敏效果，纳米复合材料具有更低的灵敏度，大致与不敏感爆炸性LLM-105的敏感性大致相当。通过热重率（Tg）和差示扫描量热计的热分析表明纳米复合材料的热分解活性高于原料的热分解活性，此外，其热稳定性更大。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18164/'>《Crystal Research and Technology: Journal of Experimental and Industrial Crystallography》</a> <b style="margin: 0 2px;">|</b><span>2018年第11期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Ping&option=202" target="_blank" rel="nofollow">Li Ping;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Kai&option=202" target="_blank" rel="nofollow">Liu Kai;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ao Denggaowa&option=202" target="_blank" rel="nofollow">Ao Denggaowa;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Xun&option=202" target="_blank" rel="nofollow">Liu Xun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xu Haifeng&option=202" target="_blank" rel="nofollow">Xu Haifeng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Duan Xiaohui&option=202" target="_blank" rel="nofollow">Duan Xiaohui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pei Chonghua&option=202" target="_blank" rel="nofollow">Pei Chonghua;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>State Key Laboratory of Environment‐friendly Energy MaterialsSouthwest University of Science and TechnologyMianyang 621010 P. R. China;</p> <p>State Key Laboratory of Environment‐friendly Energy MaterialsSouthwest University of Science and TechnologyMianyang 621010 P. R. China;</p> <p>State Key Laboratory of Environment‐friendly Energy MaterialsSouthwest University of Science and TechnologyMianyang 621010 P. R. China;</p> <p>State Key Laboratory of Environment‐friendly Energy MaterialsSouthwest University of Science and TechnologyMianyang 621010 P. R. China;</p> <p>State Key Laboratory of Environment‐friendly Energy MaterialsSouthwest University of Science and TechnologyMianyang 621010 P. R. China;</p> <p>State Key Laboratory of Environment‐friendly Energy MaterialsSouthwest University of Science and TechnologyMianyang 621010 P. R. China;</p> <p>State Key Laboratory of Environment‐friendly Energy MaterialsSouthwest University of Science and TechnologyMianyang 621010 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/160.html" title="晶体学">晶体学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=CL‐20&option=203" rel="nofollow">CL‐20;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=low sensitivity&option=203" rel="nofollow">low sensitivity;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanocomposite&option=203" rel="nofollow">nanocomposite;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanosheets&option=203" rel="nofollow">nanosheets;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=TATB&option=203" rel="nofollow">TATB;</a> </p> <div class="translation"> 机译：CL-20;低灵敏度;纳米复合材料;纳米液;TATB; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022450674.html">A Low‐Sensitivity Nanocomposite of CL‐20 and TATB</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=赵珊珊&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,赵珊珊</a> <span> <a href="/journal-cn-21562/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 兵器装备工程学报 </a> </span> <span> . 2018</span><span>,第008期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_initiators-pyrotechnics_thesis/0201226968477.html">TATB原位包覆 CL-20的研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=董璐阳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 董璐阳</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=盛涤伦&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,盛涤伦</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈利魁&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈利魁</a> <span> <a href="/journal-cn-8322/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 火工品 </a> </span> <span> . 2016</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-425_thesis/02022932403.html">CL-20/TATB复合体系的分子动力学研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZHANG Guo-ying&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . ZHANG Guo-ying</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张国英&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张国英</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=XU Rui&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,XU Rui</a> <span> <a href="/conference-cn-425/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第八届全国强动载效应及防护学术会议暨复杂介质/结构的动态力学行为创新研究群体学术研讨会 </a> <span> <span> . 2016</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020313834083.html">CL-20晶习研究及CL-20/TATB共晶的分子动力学模拟</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=文国&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 文国</a> <span> . 2014</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120101267450.html">采用乳液破乳法制备CL-20/TATB基复合含能材料的方法</a> <b>[P]</b> . <span> 中国专利： CN110423182A </span> <span> . 2019-11-08</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061204827191.html">一种微波通信用高导热系数低介电损耗聚合物基纳米复合材料的制备方法</a> <b>[P]</b> . <span> 中国专利： CN112961452B </span> <span> . 2021.12.10</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130415405891.html">Hollow nanoparticles and nanocomposites and methods of making hollow nanoparticles and nanocomposites</a> <b>[P]</b> . <span> 外国专利：  US9040157B2 </span> <span> . 2015-05-26</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：空心纳米颗粒和纳米复合材料以及制备空心纳米颗粒和纳米复合材料的方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130423312235.html">HOLLOW NANOPARTICLES AND NANOCOMPOSITES AND METHODS OF MAKING HOLLOW NANOPARTICLES AND NANOCOMPOSITES</a> <b>[P]</b> . <span> 外国专利：  US2011311822A1 </span> <span> . 2011-12-22</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：空心纳米颗粒和纳米复合材料以及制备空心纳米颗粒和纳米复合材料的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130433956962.html">Particles of explosive in crystalline form useful as explosive particles, e.g. nitramines, or CL20 having variable sensitivity to shock, have specified volume fraction of closed pores</a> <b>[P]</b> . <span> 外国专利：  FR2899970A1 </span> <span> . 2007-10-19</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：结晶形式的炸药颗粒可用作炸药颗粒，例如炸药。对震动敏感度不同的硝胺或CL20具有指定的封闭孔体积分数 </span> </p> </li> </ul> </div> </div> </div> <div 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