Rational Design of a Water‐Storable Hierarchical Architecture Decorated with Amorphous Barium Oxide and Nickel Nanoparticles as a Solid Oxide Fuel Cell Anode with Excellent Sulfur Tolerance

Song Yufei; Wang Wei; Ge Lei; Xu Xiaomin; Zhang Zhenbao; Juli?o Paulo Sérgio Barros; Zhou Wei; Shao Zongping

摘要

Abstract > Solid oxide fuel cells (SOFCs), which can directly convert chemical energy stored in fuels into electric power, represent a useful technology for a more sustainable future. They are particularly attractive given that they can be easily integrated into the currently available fossil fuel infrastructure to realize an ideal clean energy system. However, the widespread use of the SOFC technology is hindered by sulfur poisoning at the anode caused by the sulfur impurities in fossil fuels. Therefore, improving the sulfur tolerance of the anode is critical for developing SOFCs for use with fossil fuels. Herein, a novel, highly active, sulfur‐tolerant anode for intermediate‐temperature SOFCs is prepared via a facile impregnation and limited reaction protocol. During synthesis, Ni nanoparticles, water‐storable BaZr <sub>0.4</sub> Ce <sub>0.4</sub> Y <sub>0.2</sub> O <sub>3?</sub> <sub>δ</sub> (BZCY) perovskite, and amorphous BaO are formed in situ and deposited on the surface of a Sm <sub>0.2</sub> Ce <sub>0.8</sub> O <sub>1.9</sub> (SDC) scaffold. More specifically, a porous SDC scaffold is impregnated with a well‐designed proton‐conducting perovskite oxide liquid precursor with the nominal composition of Ba(Zr <sub>0.4</sub> Ce <sub>0.4</sub> Y <sub>0.2</sub> ) <sub>0.8</sub> Ni <sub>0.2</sub> O <sub>3?</sub> <sub>δ</sub> (BZCYN), calcined and reduced in hydrogen. The as‐synthesized hierarchical architecture exhibits high H <sub>2</sub> electro‐oxidation activity, excellent operational stability, superior sulfur tolerance, and good thermal cyclability. This work demonstrates the potential of combining nanocatalysts and water‐storable materials in advanced electrocatalysts for SOFCs. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>抽象</ title> > 固体氧化物燃料电池（SOFC）可以直接将储存在燃料中的化学能量转换为电力，代表更可持续的未来的有用技术。它们特别有吸引力，因为它们可以很容易地集成到目前可用的化石燃料基础设施中以实现理想的清洁能源系统。然而，通过化石燃料中的硫杂质引起的阳极在阳极上受到广泛使用的SOFC技术。因此，提高阳极的硫耐受对于开发与化石燃料一起使用的SOFC至关重要。本文，通过容易浸渍和有限反应方案制备用于中温SOFC的新型，高活性的硫可耐性阳极。在合成期间，Ni纳米粒子，水上储存的Bazr <sub> 0.4 </ sub> ce <sub> 0.4 </ sub> y <sub> 0.2 </ sub> O. <sub> 3？</ sub> <sub>Δ</ sub> </ i> （BZCY）Perovskite，无定形BaO在原位形成并沉积在SM的表面上 <sub> 0.2 </ sub> ce <sub> 0.8 </ sub> O. <sub> 1.9 </ sub> （SDC）脚手架。更具体地，浸渍多孔SDC支架用良好设计的质子传导钙钛矿氧化物液体前体，具有标称组成的Ba（Zr <sub> 0.4 </ sub> ce <sub> 0.4 </ sub> y <sub> 0.2 </ sub> 的） <sub> 0.8 </ sub> 你 <sub> 0.2 </ sub> O. <sub> 3？</ sub> <sub>Δ</ sub> </ i> （BZCYN），煅烧和减少氢气。 AS合成的分层架构呈现高H. <sub> 2 </ sub> 电氧化活性，优异的操作稳定性，优质硫耐受性，以及良好的热环度性。这项工作表明，在用于SOFC的先进电催化剂中将纳米催化剂和可水储存材料组合的潜力。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2017年第11期</span><b style="margin: 0 2px;">|</b><span>共1页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Song Yufei&option=202" target="_blank" rel="nofollow">Song Yufei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Wei&option=202" target="_blank" rel="nofollow">Wang Wei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ge Lei&option=202" target="_blank" rel="nofollow">Ge Lei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xu Xiaomin&option=202" target="_blank" rel="nofollow">Xu Xiaomin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Zhenbao&option=202" target="_blank" rel="nofollow">Zhang Zhenbao;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Juli?o Paulo Sérgio Barros&option=202" target="_blank" rel="nofollow">Juli?o Paulo Sérgio Barros;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhou Wei&option=202" target="_blank" rel="nofollow">Zhou Wei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shao Zongping&option=202" target="_blank" rel="nofollow">Shao Zongping;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>State Key Laboratory of Materials‐Oriented Chemical EngineeringNanjing Tech UniversityNo. 5 Xin Mofan Road Nanjing 210009 P. R. China;</p> <p>Department of Chemical EngineeringCurtin UniversityPerth Western Australia 6845 Australia;</p> <p>Center for Future MaterialsUniversity of Southern QueenslandSpringfield Central Queensland 4300 Australia;</p> <p>Department of Chemical EngineeringCurtin UniversityPerth Western Australia 6845 Australia;</p> <p>State Key Laboratory of Materials‐Oriented Chemical EngineeringNanjing Tech UniversityNo. 5 Xin Mofan Road Nanjing 210009 P. R. China;</p> <p>Department of Chemical EngineeringCurtin UniversityPerth Western Australia 6845 Australia;</p> <p>State Key Laboratory of Materials‐Oriented Chemical EngineeringNanjing Tech UniversityNo. 5 Xin Mofan Road Nanjing 210009 P. R. China;</p> <p>Department of Chemical EngineeringCurtin UniversityPerth Western Australia 6845 Australia;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=anode&option=203" rel="nofollow">anode;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=energy conversion&option=203" rel="nofollow">energy conversion;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solid oxide fuel cells&option=203" rel="nofollow">solid oxide fuel cells;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=sulfur tolerance&option=203" rel="nofollow">sulfur tolerance;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=water‐storable material&option=203" rel="nofollow">water‐storable material;</a> </p> <div class="translation"> 机译：阳极;能量转换;固体氧化物燃料电池;硫耐受性;可储水材料; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-foreign_detail_thesis/0204114641033.html">Rational Design of a 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Final Report for October 1, 2004 to December 31, 2008</a> <b>[R] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang, L.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Yang, L.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu, M.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Liu, M. </a> <span>2009</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于固体氧化物燃料电池的新型耐硫阳极。 2004年10月1日至2008年12月31日的最终报告</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_acta-physico-chimica-sinica_thesis/0201280470129.html">具有优异甲醇耐受性的Rh掺杂PdCu有序金属间化合物纳米粒子增强氧还原电催化</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李蒙刚&option=202" target="_blank" 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rel="nofollow" class="tuijian_auth tuijian_authcolor">,钟巍</a> <span> <a href="/journal-cn-9125/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 广州化工 </a> </span> <span> . 2016</span><span>,第005期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_journal-chemical-physics_thesis/0201296589100.html">基于多物理场模拟的低水甲烷燃料固体氧化物燃料电池的抗积碳阳极设计（英文）</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=朱江&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 朱江</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王宝轩&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王宝轩</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=林子敬&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,林子敬</a> <span> <a href="/journal-cn-12046/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 化学物理学报 </a> </span> <span> . 2018</span><span>,第5期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_renewable-energy-resources_thesis/0201228558069.html">具有闭塞端阳极的燃料电池内液态水积聚研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=叶文&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 叶文</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=叶强&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,叶强</a> <span> <a href="/journal-cn-8394/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 可再生能源 </a> </span> <span> . 2012</span><span>,第011期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020311538864.html">镓酸镧基固体氧化物燃料电池镍-铁-镓酸镧复合阳极的研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=贺琼&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 贺琼</a> <span> . 2007</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120105160682.html">用于固体氧化物燃料电池的基于镍泡沫和毡的阳极</a> <b>[P]</b> . <span> 中国专利： CN1961443A </span> <span> . 2007-05-09</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120101847402.html">一种硫氧固体氧化物燃料电池阳极材料</a> <b>[P]</b> . <span> 中国专利： CN103117399A </span> <span> . 2013-05-22</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130417913020.html">Nickel oxide powder material for solid oxide type fuel cell and method for producing the same, and anode material, anode and solid oxide type fuel cell using the same</a> <b>[P]</b> . <span> 外国专利：  US8741502B2 </span> <span> . 2014-06-03</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于固体氧化物型燃料电池的氧化镍粉末材料及其制造方法，以及使用该材料的阳极材料，阳极和固体氧化物型燃料电池 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130418173132.html">NICKEL OXIDE POWDER MATERIAL FOR SOLID OXIDE TYPE FUEL CELL AND METHOD FOR PRODUCING THE SAME, AND ANODE MATERIAL, ANODE AND SOLID OXIDE TYPE FUEL CELL USING THE SAME</a> <b>[P]</b> . <span> 外国专利：  US2013309399A1 </span> <span> . 2013-11-21</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于固体氧化物型燃料电池的氧化镍粉末材料及其制备方法，以及使用相同物质的阳极材料，阳极和固体氧化物型燃料电池 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130428287182.html">NICKEL OXIDE POWDER MATERIAL FOR SOLID OXIDE TYPE FUEL CELL AND METHOD FOR PRODUCING THE SAME, AND ANODE MATERIAL, ANODE AND SOLID OXIDE TYPE FUEL CELL USING THE SAME</a> <b>[P]</b> . <span> 外国专利：  US2010221640A1 </span> <span> . 2010-09-02</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于固体氧化物型燃料电池的氧化镍粉末材料及其制备方法，以及使用相同物质的阳极材料，阳极和固体氧化物型燃料电池 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704022435657','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" 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