High‐Pressure High‐Temperature Transparent Fixed‐Bed Reactor for Operando Gas‐Liquid Reaction Follow‐up

De Sousa Duarte Marisa; Rolland Matthieu; Sagnard Corinne; Suire Didier; Flacher Frederic; Delpoux Olivier; Lienemann Charles P.

摘要

Abstract >A 3‐MPa, 350?°C fixed‐bed reactor was designed to follow‐up gas‐liquid‐solid reactions on a millimetric size heterogeneous catalyst with Raman spectroscopy. The transparent reactor is a quartz cylinder enclosed in a Joule effect heated stainless‐steel tube. A methodology to determine how to focus the microscope for liquid and solid phase characterization is presented. The setup was validated by performing diesel hydrodesulfurization on a CoMo/alumina extrudate catalyst with a conversion very close to expected values along with the acquisition of Raman spectra of the solid catalyst showing an evolution of the catalyst phase during sulfidation. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 350℃，350°C固定床反应器设计用于用拉曼光谱对毫米尺寸的非均相催化剂进行随访的气液固体反应。透明反应器是一种封闭在焦耳效果加热的不锈钢管中的石英圆筒。提出了一种方法，以确定如何聚焦显微镜的液体和固相表征。通过在COMO /氧化铝挤出物催化剂上对COMO /氧化铝挤出物催化剂进行柴油加氢钠进行验证，以及在硫化过程中的催化剂相的进化中获取的转化率以及用于催化剂相的演变的RAMAN光谱的转化率验证。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16566/'>《Chemical Engineering & Technology: Industrial Chemistry -Plant Equipment -Process Engineering -Biotechnology》</a> <b style="margin: 0 2px;">|</b><span>2019年第3期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=De Sousa Duarte Marisa&option=202" target="_blank" rel="nofollow">De Sousa Duarte Marisa;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rolland Matthieu&option=202" target="_blank" rel="nofollow">Rolland Matthieu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sagnard Corinne&option=202" target="_blank" rel="nofollow">Sagnard Corinne;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Suire Didier&option=202" target="_blank" rel="nofollow">Suire Didier;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Flacher Frederic&option=202" target="_blank" rel="nofollow">Flacher Frederic;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Delpoux Olivier&option=202" target="_blank" rel="nofollow">Delpoux Olivier;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lienemann Charles P.&option=202" target="_blank" rel="nofollow">Lienemann Charles P.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>IFP Energies nouvellesRond-point de l'échangeur de Solaize BP3 69360 Solaize France;</p> <p>IFP Energies nouvellesRond-point de l'échangeur de Solaize BP3 69360 Solaize France;</p> <p>IFP Energies nouvellesRond-point de l'échangeur de Solaize BP3 69360 Solaize France;</p> <p>IFP Energies nouvellesRond-point de l'échangeur de Solaize BP3 69360 Solaize France;</p> <p>IFP Energies nouvellesRond-point de l'échangeur de Solaize BP3 69360 Solaize France;</p> <p>IFP Energies nouvellesRond-point de l'échangeur de Solaize BP3 69360 Solaize France;</p> <p>IFP Energies nouvellesRond-point de l'échangeur de Solaize BP3 69360 Solaize France;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/238.html" title="化学工业">化学工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Diesel hydrodesulfurization&option=203" rel="nofollow">Diesel hydrodesulfurization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fixed‐bed reactor&option=203" rel="nofollow">Fixed‐bed reactor;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gas‐liquid reactions&option=203" rel="nofollow">Gas‐liquid reactions;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Operando Raman spectroscopy&option=203" rel="nofollow">Operando Raman spectroscopy;</a> </p> <div class="translation"> 机译：柴油加氢脱硫;固定床反应器;气液反应;操作型拉曼光谱; 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=史士东&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,史士东</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李文博&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李文博</a> <span> <a href="/conference-cn-14314/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 2010中国新型煤化工发展及示范项目进展论坛 </a> <span> <span> . 2010</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020312600182.html">气液共进料的高通量固定床反应器的研究和在催化反应中的应用</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=邱枫&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 邱枫</a> <span> . 2009</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120103280295.html">一种高温高压固定床反应器</a> <b>[P]</b> . <span> 中国专利： CN110801788A </span> <span> . 2020-02-18</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120211416382.html">一种高温高压固定床反应器</a> <b>[P]</b> . <span> 中国专利： CN211384942U </span> <span> . 2020-09-01</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130409499306.html">Method for obtaining synthesis gas through gasification of residual liquids with the ashes of fixed bed gasification at a pressure of between 0.3 and 8.0 MPa and a temperature higher than 1400 u00b0 C with gas rich in oxygen in a reactor gassing refrigerated</a> <b>[P]</b> . <span> 外国专利：  BR112012005838A2 </span> <span> . 2017-05-30</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过在固定反应器中将残余液体气化，在0.3和8.0 MPa之间的压力下，在高于1400 oC的温度下用富含氧气的气体在冷冻反应器中充气来气化残余液体的方法来获得合成气 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130422006036.html">METHOD FOR SELECTIVELY ELIMINATING SULFUR COMPONENTS FROM BIOMASS-BASED SYNGAS USING ROOM TEMPERATURE-BASED IONIC LIQUID CAPABLE OF EASILY CONTROLLING EXOTHERMIC PHENOMENON IN A FIXED BED CATALYTIC REACTOR-BASED FISCHER-TROPSCH REACTION</a> <b>[P]</b> . <span> 外国专利：  KR20120094628A </span> <span> . 2012-08-27</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：在固定床催化反应器的FISCHER-TROPSCH反应中使用基于室温的离子液体能够轻松控制放热现象的方法，从生物量为基础的SYNGAS中选择性消除硫的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130437788924.html">Trickling Bed Reactor adapted to oxidize a SOLUTE in the liquid Phase; Trickling Bed Reactor adapted for gas - Liquid reaction method; to optimize the performance ofBoth Reactors, and the Reactor adapted to oxidize a Liquid by varying The Geometry of the Reaction column.</a> <b>[P]</b> . <span> 外国专利：  CL2004002628A1 </span> <span> . 2006-03-24</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：滴流床反应器，适于氧化液相中的溶质;适用于气体的滴流床反应器-液体反应方法;以优化两个反应器的性能，并且该反应器通过改变反应塔的几何形状而适合于氧化液体。 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704022180998','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="关闭" onclick="$('.journalsub-pop-up').hide()"> 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