Novel chiral ionic liquids stationary phases for the enantiomer separation of chiral acid by high‐performance liquid chromatography

机译：新型手性离子液体静止相对于高效液相色谱法分离手性液相传阶段

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Abstract >Novel chiral ionic liquid stationary phases based on chiral imidazolium were prepared. The ionic liquid chiral selector was synthesized by ring opening of cyclohexene oxide with imidazole or 5,6‐dimethylbenzimidazole, and then chemically modified by different substitute groups. Chiral stationary phases were prepared by bonding to the surface of silica sphere through thioene “click” reaction. Their enantioselective separations of chiral acids were evaluated by high‐performance liquid chromatography. The retention of acid sample was related to the counterion concentration and showed a typical ion exchange process. The chiral separation abilities of chiral stationary phases were greatly influenced by the substituent group on the chiral selector as well as the mobile phase, which indicated that, besides ion exchange, other interactions such as steric hindrance, π‐π interaction, and hydrogen bonding are important for the enantioselectivity. In this report, the influence of bulk solvent components, the effects of varying concentration, and the type of the counterion as well as the proportion of acid and basic additives were investigated in detail. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“En”> <标题类型=“main”>摘要</标题> >基于手性咪唑鎓的新型手性离子液体固定阶段。通过与咪唑或5,6-二甲基双咪唑的环己烯开环合成离子液体手性选择器，然后通过不同的替代组化学改性。通过通过噻烯“点击”反应将通过二氧化硅球的表面键合来制备手性固定相。通过高效液相色谱法评估其对肾上腺酸的对映选择性分离。酸样品的保留与抗衡离子浓度有关并显示出典型的离子交换过程。手性固定相的手性分离能力受手动选择器上的取代基以及流动相的影响，表明除了离子交换之外，还具有空间障碍，π-π相互作用等其他相互作用对映射性很重要。在本报告中，详细研究了本体溶剂组分，不同浓度的影响以及抗衡浓度的效果以及酸和碱性添加剂的比例。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16290/'>《Chirality: The pharmacological, biological, and chemical consequences of molecular asymmetry》</a> <b style="margin: 0 2px;">|</b><span>2018年第5期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=He Shanshan&option=202" target="_blank" rel="nofollow">He Shanshan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=He Yunchao&option=202" target="_blank" rel="nofollow">He Yunchao;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cheng Lingping&option=202" target="_blank" rel="nofollow">Cheng Lingping;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Yaling&option=202" target="_blank" rel="nofollow">Wu Yaling;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ke Yanxiong&option=202" target="_blank" rel="nofollow">Ke Yanxiong;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Engineering Research Center of Pharmaceutical Process Chemistry School of Pharmacy Ministry of EducationEast China University of Science and TechnologyShanghai China;</p> <p>Engineering Research Center of Pharmaceutical Process Chemistry School of Pharmacy Ministry of EducationEast China University of Science and TechnologyShanghai China;</p> <p>Engineering Research Center of Pharmaceutical Process Chemistry School of Pharmacy Ministry of EducationEast China University of Science and TechnologyShanghai China;</p> <p>Engineering Research Center of Pharmaceutical Process Chemistry School of Pharmacy Ministry of EducationEast China University of Science and TechnologyShanghai China;</p> <p>Engineering Research Center of Pharmaceutical Process Chemistry School of Pharmacy Ministry of EducationEast China University of Science and TechnologyShanghai China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4812.html" title="结构化学">结构化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=5&option=203" rel="nofollow">5;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=6‐dimethylbenzimidazole&option=203" rel="nofollow">6‐dimethylbenzimidazole;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=anion‐exchange&option=203" rel="nofollow">anion‐exchange;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=cyclohexene oxide&option=203" rel="nofollow">cyclohexene oxide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=enantioselectivity&option=203" rel="nofollow">enantioselectivity;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hydrogen bonding&option=203" rel="nofollow">hydrogen bonding;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=imidazolium&option=203" rel="nofollow">imidazolium;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=substituent group&option=203" rel="nofollow">substituent group;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=π‐π interaction&option=203" rel="nofollow">π‐π interaction;</a> </p> <div class="translation"> 机译：5;6-二甲基双咪唑;阴离子交换;环己烯;对致氢键;氢键;咪唑鎓;取代基;π-π相互作用; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022113568.html">Novel chiral ionic liquids stationary phases for the enantiomer separation of chiral acid by high‐performance liquid chromatography</a> <b>[J]</b> . <span> <a 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=方骏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 方骏</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=夏小庆&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,夏小庆</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴勇勇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,吴勇勇</a> <span> <a href="/journal-cn-6431/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国药物化学杂志 </a> </span> <span> . 2003</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-chromatography_thesis/0201247008791.html">α-苯乙醇对映体在涂敷三苯甲酸纤维素酯手性固定相上的高效液相色谱法分离—洗脱液中醇的影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王来来&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王来来</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吕士杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,吕士杰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=高平&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,高平</a> <span> <a href="/journal-cn-14390/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 色谱 </a> </span> <span> . 1999</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-20922_thesis/02022232240.html">新型含苯并噻唑基α-氨基磷酸酯类化合物的高效液相手性固定相分离方法研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=卢平&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 卢平</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=薛伟&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,薛伟</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张钰萍&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张钰萍</a> <span> <a href="/conference-cn-20922/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第七届全国新农药创制学术交流会 </a> <span> <span> . 2007</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020313802076.html">基于手性离子液体的毛细管电泳技术在手性氨基酸分离中的应用研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴玉娇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 吴玉娇</a> <span> . 2014</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120103428377.html">一种用高效液相色谱法分离测定含多个手性中心的多肽手性异构体的方法</a> <b>[P]</b> . <span> 中国专利： CN110702819A </span> <span> . 2020-01-17</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120113803436.html">手性检测装置、手性检测方法、分离装置、分离方法和手性物质装置</a> <b>[P]</b> . <span> 中国专利： CN113826003A </span> <span> . 2021-12-21</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130442387583.html">Chiral stationary phases are based on terpenoids, are of brush type used in separation of enantiomers by high efficiency liquid chromatography</a> <b>[P]</b> . <span> 外国专利：  PT102878A </span> <span> . 2004-05-31</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：手性固定相基于萜类化合物，是通过高效液相色谱法分离对映异构体所用的刷型固定相 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130458337408.html">Method for separating enantiomers on chiral stationary phases by liquid chromatography in capillary columns</a> <b>[P]</b> . <span> 外国专利：  DE4413121A1 </span> <span> . 1995-02-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：毛细管柱液相色谱在手性固定相上分离对映体的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130438920861.html">Chiral stationary phase and chiral mobile phase, useful for analytical or preparative separation of enantiomers, includes an oligonucleotide with specific affinity as chiral selector</a> <b>[P]</b> . <span> 外国专利：  FR2855822A1 </span> <span> . 2004-12-10</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于对映异构体的分析或制备分离的手性固定相和手性流动相包括具有特定亲和力的寡核苷酸作为手性选择剂 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div 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