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Cationic Vacancy Defects in Iron Phosphide: A Promising Route toward Efficient and Stable Hydrogen Evolution by Electrochemical Water Splitting

机译：磷化铁中的阳离子空位缺陷：电化学水分裂有效且稳定的氢气进化的有希望的路线

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Abstract > Engineering the electronic properties of transition metal phosphides has shown great effectiveness in improving their intrinsic catalytic activity for the hydrogen evolution reaction (HER) in water splitting applications. Herein, we report for the first time, the creation of Fe vacancies as an approach to modulate the electronic structure of iron phosphide (FeP). The Fe vacancies were produced by chemical leaching of Mg that was introduced into FeP as “sacrificial dopant”. The obtained Fevacancy‐rich FeP nanoparticulate films, which were deposited on Ti foil, show excellent HER activity compared to pristine FeP and Mg‐doped FeP, achieving a current density of 10?mA?cm ?2 at overpotentials of 108?mV in 1? <sc>m</sc> KOH and 65?mV in 0.5? <sc>m</sc> H <sub>2</sub> SO <sub>4</sub> , with a near‐100?% Faradaic efficiency. Our theoretical and experimental analyses reveal that the improved HER activity originates from the presence of Fe vacancies, which lead to a synergistic modulation of the structural and electronic properties that result in a near‐optimal hydrogen adsorption free energy and enhanced proton trapping. The success in catalytic improvement through the introduction of cationic vacancy defects has not only demonstrated the potential of Fe‐vacancy‐rich FeP as highly efficient, earth abundant HER catalyst, but also opens up an exciting pathway for activating other promising catalysts for electrochemical water splitting. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 工程过渡金属磷化磷酸的电子性质在改善水分裂应用中提高氢进化反应（她）的内在催化活性方面具有很大的有效性。在此，我们首次报告，产生FE职位空缺作为调节铁磷的电子结构的方法（FEP）。 FE职位空缺是通过将Mg的化学浸出产生的，所述MG被引入FEP中作为“牺牲掺杂剂”。与原始FEP和Mg掺杂的FEP相比，所获得的富含FEP的FEP纳米颗粒膜沉积在Ti箔上，呈现出优异的活性，并且达到电流密度为10？ma？cm ？2 </ sup> 在108的过电容器中1？ <sc> m </ sc> KOH和65？MV 0.5？ <sc> m </ sc> H <sub> 2 </ sub> 所以 <sub> 4 </ sub> ，近100岁的竞争效率。我们的理论和实验分析表明，改善的她的活动源于FE空位的存在，这导致结构和电子性质的协同调节，从而导致近最佳的氢吸附自由能量和增强的质子捕获。通过引入阳离子空位缺陷的催化改善的成功不仅证明了Fe空空位的FEP潜在的潜力，而且对其催化剂充满了富有效率，而且还为激活了用于激活用于电化学水分裂的其他有希望的催化剂的激动途径。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16185/'>《ChemSusChem》</a> <b style="margin: 0 2px;">|</b><span>2017年第22期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kwong Wai Ling&option=202" target="_blank" rel="nofollow">Kwong Wai Ling;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gracia‐Espino Eduardo&option=202" target="_blank" rel="nofollow">Gracia‐Espino Eduardo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lee Cheng Choo&option=202" target="_blank" rel="nofollow">Lee Cheng Choo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sandstr?m Robin&option=202" target="_blank" rel="nofollow">Sandstr?m Robin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=W?gberg Thomas&option=202" target="_blank" rel="nofollow">W?gberg Thomas;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Messinger Johannes&option=202" target="_blank" rel="nofollow">Messinger Johannes;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryUme? University90187 Ume? Sweden;</p> <p>Department of PhysicsUme? University90187 Ume? Sweden;</p> <p>Ume? Core Facility for Electron MicroscopyUme? University90187 Ume? Sweden;</p> <p>Department of PhysicsUme? University90187 Ume? Sweden;</p> <p>Department of PhysicsUme? University90187 Ume? Sweden;</p> <p>Department of ChemistryUme? University90187 Ume? Sweden;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=artificial photosynthesis&option=203" rel="nofollow">artificial photosynthesis;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=cation vacancy&option=203" rel="nofollow">cation vacancy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=iron phosphide&option=203" rel="nofollow">iron phosphide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=sacrificial dopant&option=203" rel="nofollow">sacrificial dopant;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solar fuels&option=203" rel="nofollow">solar fuels;</a> </p> <div class="translation"> 机译：人造光合作用;阳离子空位;磷化铁;牺牲掺杂剂;太阳能燃料; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022092260.html">Cationic Vacancy Defects in Iron Phosphide: A Promising Route toward Efficient and Stable Hydrogen Evolution by Electrochemical Water Splitting</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kwong Wai Ling&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Kwong Wai Ling,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gracia‐Espino Eduardo&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Gracia‐Espino Eduardo,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lee Cheng Choo&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Lee Cheng Choo,</a> <a href="/journal-foreign-16185/" target="_blank" rel="nofollow" class="tuijian_authcolor">ChemSusChem .</a> <span>2017</span><span>,第22期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：磷化铁中的阳离子空位缺陷：电化学水分裂有效且稳定的氢气进化的有希望的路线</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704020629714.html">Self-growth Ni2P nanosheet arrays with cationic vacancy defects as a highly efficient bifunctional electrocatalyst for overall water splitting</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> </a> <a href="/journal-foreign-33995/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of Colloid and Interface Science .</a> <span>2020</span><span>,第期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：自我生长Ni2P纳米片阵列具有阳离子空位缺陷作为整体水分裂的高效双官能电催化剂</span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704020693763.html">Microwave-assisted ultrafast synthesis of adjustable bimetal phosphide/graphene heterostructures from MOFs for efficient electrochemical water splitting</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bu Fanxing&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Bu Fanxing,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Wenshu&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Chen Wenshu,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aboud Mohamed F. 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