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Evaluation of the thermal shock resistance of aluminate-silicate refractory castables. Effect of the thermal treatment

机译:铝酸盐硅酸盐耐火浇铸件的热抗冲击性评价。 热处理的影响

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In this work, the thermal shock response of commercial fireclay refractory castable with low alumina content was analyzed with the aim of evaluating the feasibility to be used as replacement of silicate-aluminate refractory bricks in a non-severe process. The study was performed in laboratory scale, with procedures especially designed based on the available standards, employing 2 commercial castables supplied by different manufacturers. Specimens cured for 24 h, 48 h and 7 days (for comparison with samples of civil concrete) were evaluated; some specimens were also thermally treated at 900 degrees C. As-received materials were characterized through granulometric analysis by sieving and X-ray diffraction. The specimens were mechanically tested in flexion and compression; moreover, the density, the porosity and the dynamic Young's modulus of the samples were measured. The thermal shock test was performed by air cooling; after each cycle, the dynamic Young's modulus was determined. At the end of the fifth cycle, the residual mechanical strength in flexion and compression was also determined. The results showed that the castable with finer granulometry and better mechanical performance before the thermal shock (castable A), was the most suitable to be used without a previous thermal treatment. (C) 2019 SECV. Published by Elsevier Espana, S.L.U.
机译:在这项工作中,分析了具有低氧化铝含量的商业火星耐火膨胀件的热冲击响应,目的是评估在非严重过程中用作硅酸盐铝酸盐耐火砖的可行性。该研究以实验室规模进行,采用根据可用标准尤其设计的程序,采用不同制造商提供的2个商业陆战队。评估标本固化24小时,48小时和7天(与民用混凝土样品相比)进行评估;一些样品在900摄氏度下也热处理。通过筛分和X射线衍射通过粒度分析表征接收的材料。在屈曲和压缩中机械测试标本;此外,测量了样品的密度,孔隙率和动态杨氏模量。通过空气冷却进行热冲击试验;在每个循环之后,确定动态杨氏模量。在第五循环结束时,还测定屈曲和压缩中的残留机械强度。结果表明,在热冲击(可浇铸A)之前,具有更精细的粒度测量和更好的机械性能,最适合使用而无需先前的热处理。 (c)2019 SECV。 elsevier espana发布,s.l.u。

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