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Local comparability of proficiency testing results: determination of concrete slump and compressive strength values

机译:能力验证结果的本地可比性:确定混凝土坍落度和抗压强度值

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摘要

A proficiency testing (PT) scheme is developed for comparability assessment of results of concrete slump and compressive strength determination. The scheme is based on preparing of a test portion/sample of a concrete in-house reference material (IHRM) at a reference laboratory (RL) in the same conditions for every PT participant. Therefore, in this scheme IHRM instability is not relevant as a source of measurement/test uncertainty, while intra- and between-samples inhomogeneity parameters are evaluated using the results of RL testing of the samples taken at the beginning, the middle and the end of the PT experiment. The IHRM assigned slump and compressive strength values are calculated as averaged RL results. Their uncertainties include the measurement/test uncertainty components and the components arising from the material inhomogeneity. The test results of 25 PT participants were compared with the IHRM assigned values taking into account both the uncertainties of the assigned values and the measurement/test uncertainties of the participants. Since traceability of the IHRM assigned values to the international measurement standards and SI units cannot be stated, local comparability of the results is assessed. It is shown, that comparability of the slump and compressive strength determination results is satisfactory, while uncertainty evaluation for slump results requires additional efforts.
机译:开发了一种能力测试(PT)方案,用于混凝土坍落度和抗压强度确定结果的可比性评估。该计划基于在每个参试人员相同条件下,在参考实验室(RL)制备混凝土内部参考材料(IHRM)的测试部分/样品的过程。因此,在该方案中,IHRM的不稳定性与测量/测试不确定性的来源无关,而样品内部和样品之间的不均匀性参数是使用在样品开始,中间和结束时进行的RL测试的结果进行评估的PT实验。 IHRM指定的坍落度和抗压强度值被计算为RL的平均结果。它们的不确定性包括测量/测试不确定性成分以及由材料不均匀性引起的成分。考虑到分配值的不确定性和参与者的测量/测试不确定性,将25名PT参与者的测试结果与IHRM分配的值进行了比较。由于无法说明IHRM分配值到国际测量标准和SI单位的可追溯性,因此要评估结果的本地可比性。结果表明,坍落度和抗压强度确定结果的可比性令人满意,而坍落度结果的不确定性评估则需要额外的努力。

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