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Facile preparation of nanosized yttrium oxide by the thermal decomposition of amorphous Schiff base yttrium complex precursor

机译:纳米化氧化钇含有无定形席铬钇钇络合物前体的纳米钇氧化物制备

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摘要

Nanoparticles of yttrium (III) oxide were synthetized by thermal combustion of previously prepared yttrium complex of pyridoxylidenealanine under air atmosphere at 750 degrees C Amorphous complex was characterized by XRD and IR and NMR spectroscopy. The prepared nanoparticles were characterized by XRD and TEM revealing the size of the vast majority of particles ranging from 10 to 30 nm. The synthesis method can be modified by addition of any RE and can be used for many applications especially in the field of non-linear optics or in biomedical applications where use of more fine nanoparticles may be problematic or even dangerous. (C) 2016 Elsevier B.V. All rights reserved.
机译:通过在空气气氛下在750℃的空气气氛下,通过先前制备的吡哆any anine的钇络合物的热燃烧合成了氧化钇(III)氧化物的纳米颗粒。通过XRD和IR和NMR光谱,特征在于750℃的无定形络合物。 通过XRD和TEM表征制备的纳米颗粒,揭示了大部分颗粒的尺寸为10至30nm。 可以通过添加任何RE来修改合成方法,并且可以用于许多应用特别是在非线性光学器件领域或在使用更细的纳米颗粒的生物医学应用中可能是有问题的甚至危险的。 (c)2016 Elsevier B.v.保留所有权利。

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