Poly( <i xmlns='http://www.wiley.com/namespaces/wiley'>NN ‐vinyl imidazole) grafted silica nanofillers: Synthesis by RAFT polymerization and nanocomposites with polybenzimidazole

Kutcherlapati Satyanarayana Raju; Koyilapu Rambabu; Jana Tushar

摘要

ABSTRACT > In this report, we synthesized poly( N ‐vinyl imidazole) (PNVI) grafted silica nanoparticles (SiNP) by using RAFT polymerization through grafting‐from approach to demonstrate that the self‐assembled structure of SiNP is the key diving force in improving physical properties of SiNP based nanocomposites. In a multistep synthetic process, well‐defined PNVI chains with tunable molecular weights and surface chain densities were grown from the RAFT agent anchored SiNP surface using N ‐vinyl imidazole (NVI) as a monomer. Spectroscopic and thermal analysis confirmed surface grafting of PNVI on SiNP surface and the amount of grafted PNVI chins were also quantified. The mean diameter of the PNVI grafted SiNP (PNVI‐ g ‐SiNP) particles altered between 50 and 100 nm with the variation of PNVI chain lengths. The present approach is metal‐catalyst free, straight forward, and provides PNVI functionalized SiNP in a simple manner in comparison to the reported methods. Further, these PNVI‐ g ‐SiNP particles were used as a nanofiller to prepare nanocomposites with Poly(4,4′‐diphenylether‐5,5′‐bibenzimidazole) (OPBI). These nanocomposites displayed significantly higher mechanical, proton conductivity and less acid leaching properties than the pristine OPBI. The anisotropic self‐assembled ordered structure formation of nanofillers in the nanocomposites believed to be the driving force for the enhanced physical properties. ? 2017 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2018 , 56 , 365–375 </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”> <title type =“main”>抽象</ title> >在本报告中，我们合成多（<通过使用筏聚合通过</ i>从</ i>从嫁接方法使用筏聚合，乙烯基咪唑（PNVI）接枝的二氧化硅纳米颗粒（SINP）证明SINP的自组装结构是关键潜水改善基于SINP纳米复合材料的物理性质的力。在多步骤合成过程中，使用可调谐分子量和表面链密度的明确定义的PNVI链，使用 N-I> - 乙烯基咪唑（NVI）作为单体，从筏剂锚定SINP表面生长。光谱和热分析证实了SINP表面上PNVI的表面接枝和嫁接的PNVI下巴的量也被定量。 PNVI接枝SINP的平均直径（PNVI- <I> G / I> -SINP）颗粒在50至100nm之间改变为PNVI链长度的变化。本方法是无金属催化剂，直接向前，并以简单的方式提供PNVI官能化SINP与报道的方法相比。此外，这些PNVI- <I> G-I> -SINP颗粒用作纳米填料，以制备具有聚（4,4'-二苯基醚-5,5,5'- Bibenzimidazole）（OPBI）的纳米复合材料。这些纳米复合材料显着更高的机械，质子电导率和少于原始OPBI的酸性浸出性能。纳米复合材料中的纳米填充物的各向异性自组装有序结构形成为增强物理性质的驱动力。还是2017 Wiley期刊，Inc.J.Colom。 SCI。，A部分：polym。化学。 2018 </ b>， 56 </ i>，365-375 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35621/'>《Journal of Polymer Science, Part A. Polymer Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2018年第4期</span><b style="margin: 0 2px;">|</b><span>共11页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kutcherlapati Satyanarayana Raju&option=202" target="_blank" rel="nofollow">Kutcherlapati Satyanarayana Raju;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Koyilapu Rambabu&option=202" target="_blank" rel="nofollow">Koyilapu Rambabu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jana Tushar&option=202" target="_blank" rel="nofollow">Jana Tushar;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of ChemistryUniversity of HyderabadTelangana 500046 India;</p> <p>School of ChemistryUniversity of HyderabadTelangana 500046 India;</p> <p>School of ChemistryUniversity of HyderabadTelangana 500046 India;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1184.html" title="有机化学">有机化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=poly( N ‐vinyl imidazole)&option=203" rel="nofollow">poly( N ‐vinyl imidazole);</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=proton exchange membranes&option=203" rel="nofollow">proton exchange membranes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=RAFT polymerization&option=203" rel="nofollow">RAFT polymerization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=self‐assembly&option=203" rel="nofollow">self‐assembly;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=silica nanoparticles&option=203" rel="nofollow">silica nanoparticles;</a> </p> <div class="translation"> 机译：聚（N-乙烯基咪唑）;质子交换膜;筏聚合;自组装;二氧化硅纳米粒子; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704020725994.html">Poly( <i xmlns="http://www.wiley.com/namespaces/wiley">NN ‐vinyl imidazole) grafted silica nanofillers: Synthesis by RAFT polymerization and nanocomposites with polybenzimidazole</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kutcherlapati Satyanarayana Raju&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Kutcherlapati Satyanarayana Raju,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Koyilapu Rambabu&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Koyilapu Rambabu,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jana Tushar&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Jana Tushar </a> <a href="/journal-foreign-35621/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of Polymer Science, Part A. 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initial;text-overflow: initial;overflow: initial;"> <span>机译：合成功能化聚（1,3-alcadienos）的方法官能化聚（1,3-alcadienos）的方法-以受控方式制备接枝到不饱和弹性体上的乙烯基芳族化合物的（CO）聚合物的方法，以及（CO）高抗冲乙烯基芳烃的聚合物。 </span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06130412227368.html">Process for the synthesis of poly (1,3 - alcadienos) functionalized poly (1,3 - alcadienos) functionalized, process for the preparation of (CO) polymers of vinyl aromatic grafted onto an unsaturated elastomer in a controlled manner, and (CO) polymer of high impact vinyl aromatic.</a> <b>[P]</b> . <span> 外国专利：  BRPI0917857A2 </span> <span> . 2015-11-24</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：聚（1,3-alcadienos）官能化聚（1,3-alcadienos）的合成方法，以可控方式接枝到不饱和弹性体上的乙烯基芳族化合物（CO）的制备方法和（CO）高抗冲乙烯基芳烃的聚合物。 </span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130487975848.html">A method for the preparation of vinyl halogen polymers, in particular of grafted poly vinyl halogen - poly olefin polymers and mixtures</a> <b>[P]</b> . <span> 外国专利：  DE1570990A1 </span> <span> . 1970-03-12</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：一种制备乙烯基卤素聚合物，特别是接枝的聚乙烯基卤素-聚烯烃聚合物及其混合物的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704020725994','4',7,2,1,'',this,24)" class="delivery" prompt="010401" 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Poly( NN ‐vinyl imidazole) grafted silica nanofillers: Synthesis by RAFT polymerization and nanocomposites with polybenzimidazole

摘要