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A Facile Strategy to Fabricate Nanoscale Zero-Valent Iron Decorated Graphene Oxide Composite for Dechloridation of Trichloroacetic Acid in Water

机译:制造纳米级零价铁的容易策略装饰石墨烯氧化物复合材料,用于水中三氯乙酸的脱氯化

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摘要

In this study, nanoscale zero-valent iron decorated graphene oxide (NZVI/GO) composite was fabricated through a reduction process in the presence of sodium borohydride (NaBH4) solution. Subsequently, physicochemical properties of the NZVI/GO composites were characterized by scanning electron microscope (SEM), transmission electron microscopy (TEM), N-2 adsorption/desorption, X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Fourier transformation infrared spectroscopy (FT-IR) and Raman spectra. Results indicated that Fe species existed in the form of Fe-0, which uniformly dispersed on the surface of GO. Furthermore, the performance of NZVI/GO was evaluated by the degradation of tichloroacetic acid (TCAA). TCAA can be rapidly degraded by NZVI/GO. This paper provides a promising strategy to synthesize versatile catalyst which would be potentially applied in sewage treatment to degrade chlorinated organic compounds.
机译:在本研究中,通过硼氢化钠(NaBH4)溶液存在的还原过程制造纳米级零价铁装饰石墨烯氧化物(NZVI / GO)复合材料。 随后,通过扫描电子显微镜(SEM),透射电子显微镜(TEM),N-2吸附/解吸,X射线衍射(XRD),X射线光电子谱(XPS),表征NZVI / GO复合材料的物理化学性质。 ,傅里叶变换红外光谱(FT-IR)和拉曼光谱。 结果表明,Fe-0形式存在Fe物种,其均匀地分散在去的表面上。 此外,通过噻氯酸(TCAA)的降解来评估NZVI / Go的性能。 TCAA可以通过NZVI / Go迅速降级。 本文提供了一种有希望的策略来合成通用催化剂,其可能应用于污水处理以降解氯化有机化合物。

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