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Aging response on the stress corrosion cracking behavior of wrought precipitation-hardened magnesium alloy

机译:锻造淬火硬化镁合金应力腐蚀开裂行为的老化反应

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摘要

Constant immersion testing and slow strain rate testing (SSRT) are conducted on wrought magnesium alloy in a 3.5 wt% NaCl solution. After solution annealing (SA) at 525 degrees C for 8 h, the alloy was isothermally aged at 210 degrees C for 15 h, 48 h, and 144 h to obtain underaged (UA), peak-aged (PA), and overaged (OA) microstructures, respectively. After 32 days of constant exposure in chloride solution, the SA and UA samples showed the lowest (similar to 0.10 mg cm(-2) day(-1)) and the highest (similar to 0.20 mg cm(-2) day(-1)) weight loss, respectively. SSRT was carried out at an initial strain rate of 10(-6) s(-1) in air and 3.5 wt% NaCl solution to investigate stress corrosion cracking (SCC) susceptibility. SCC susceptibility index was in the order PA > UA > SA > OA. Intergranular failure morphology on the fractured surface after SSRT in chloride solution can be attributed to micro-galvanic activity between grain boundary second phase and adjacent regions. Comparison of electrochemical measurements in unstressed and stressed conditions indicated two orders of magnitude difference in electrochemical resistance of the alloy.
机译:在3.5wt%NaCl溶液中对锻镁合金进行恒定的浸渍测试和慢速率测试(SSRT)。在825℃下溶液退火(SA)8小时后,该合金在210℃下等温,持续15小时,48小时,144小时,以获得未造成的(UA),峰值(PA)和occorged( OA)微观结构。在氯化物溶液中恒定暴露32天后,SA和UA样品显示最低(类似于0.10mg cm(-2)天(-1)),最高(类似于0.20mg cm(-2)天( - 1))分别减肥。 SSRT在空气中的10(-6)S(-1)的初始应变率和3.5wt%NaCl溶液中进行,以研究应力腐蚀裂解(SCC)易感性。 SCC敏感性指数是在PA> UA> SA> OA的顺序中。氯化物溶液中SSRT后裂缝表面上的晶体失效形态可归因于晶界第二阶段和相邻区域之间的微电催化活性。在不受重视和应力条件下的电化学测量比较表明了合金电化学抗性的两个峰值差。

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  • 来源
    《Journal of Materials Science》 |2020年第3期|共15页
  • 作者单位

    Missouri Univ Sci &

    Technol Ctr Frict Stir Proc Rolla MO 65409 USA;

    Indian Inst Technol Madras Dept Mech Engn Chennai 600036 Tamil Nadu India;

    Univ North Texas Dept Mat Sci &

    Engn Denton TX 76203 USA;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 工程材料学;
  • 关键词

  • 入库时间 2022-08-19 19:37:40

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