Grain- to multiple-grain-scale deformation processes during diffusion creep of forsterite plus diopside aggregate: 1. Direct observations

摘要

We uniaxially deformed fine-grained (similar to 1 mu) forsterite + diopside (5 and 20vol %) aggregates in the diffusion creep regime. Prior to deformation, line markers were milled on a lateral surface of a cylindrical sample to detect single- to multiple-grain-scale deformation. We performed deformation experiments and observations of the marker-etched surface after sample cooling multiple times on the same specimens. The strain measured at the scale of several tens of grains from macroscopic shortening of the markers parallel to the compression axis is consistent with the total strain of the sample. However, microscopically, the markers are intensely segmented and rotated at the grain scale increasing with the sample strain. Meanwhile, essentially, no deformation is observed within the grains in most of the samples. The surface microstructures, including the deformation of the markers, reveal the serial operations of grain boundary migration, grain boundary sliding, rigid body grain rotation, and grain neighbor switching, which correspond well to processes expected in diffusion-controlled superplasticity. This sequence is commonly observed in both samples consisting of forsterite grains of tabular and equiaxed grain shapes, which have been shown to develop notable crystallographic preferred orientation (CPO) and random (or weak) CPO, respectively, during diffusion creep. Intragranular regions of relatively larger forsterite grains in the specimens deformed at stresses near the transition between deformation mechanisms from diffusion creep to dislocation creep reveal marker deformation and formation of surface creases and subgrain boundaries, which indicate intragranular dislocation processes. Overall, the surface microstructures reflect the deformation state of the materials well.