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Impact of surface ultrasonic rolling on cavitation erosion behavior of 304 stainless steel

机译:表面超声波轧制对304不锈钢空化腐蚀行为的影响

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摘要

Surface ultrasonic rolling process (SURF) is a prior self-nano-technology of surface strengthening to improve the cavitation resistance of metal materials. In the paper, the 304 stainless steel (304SS) specimens were processed into 5 times, 10 times, 15 times and 20 times by SURP, then were cut into pieces along the SURP surface. In order to investigate impact of SURF on cavitation erosion behavior of 304SS, microstructure, mechanical properties and phase distribution of 304SS with difference SURP times were characterized firstly. Subsequently, ultrasonic cavitation erosion process and electrochemical measurements was experimented respectively: the specimens with different SURP times were subjected to 3 h in ore pulp solution (The mass fraction of 3.5% NaCl and 5% plumbum-zinc) by ultrasonic cavitation erosion process (UCEP), meanwhile, the electrochemical behaviors of the 304SS specimens with difference SURP times, such as open circuit potential (OCP), polarization curves and electrochemical impedance spectroscopy (EIS) were measured successively. Finally, the influences of the mechanical properties and corrosion characteristics of the 304SS with different microstructures after SURP on cavitation corrosion resistance were discussed in details, in the meantime, the microscopic mechanisms of the cavitation resistance for 304SS with different SURP times were investigated. The result shows that SURP is significantly beneficial to protect 304SS from the cavitation erosion behavior via introduction of deformation layers, transformation between martensite and austenitic, formation of passivation film, grain refinement and the surface hardness as well as residual stress of the 304SS were enhanced accordingly. However, the energy transfer of SURP is not only used to surface hardening, grain refinement, slip bands establishment but also defects formation, overmuch energy transfer plays the opposite role. Therefore SURP 10 times is a suitable SURP times that makes 304SS achieved optimal cavitation resistance.
机译:表面超声波轧制工艺(冲浪)是一种现有的自纳技术,表面强化,以改善金属材料的空化阻力。在本文中,将304个不锈钢(304SS)标本加工成5次,10倍,15倍,15倍和20次通过SURP,然后沿着SURP表面切成块。为了调查冲浪对304s的空化糜烂行为的影响,首先表现了304Ss的微观结构,机械性能和相相分布的304ss。随后,通过超声波空化腐蚀过程分别进行超声波空化腐蚀过程和电化学测量,在矿石腐浆溶液(3.5%NaCl和5%NaCl和5%NaClumum-zinc的质量分数不同的情况下,所述样品(UCEP [同时,同时,连续测量304SS样品的304SS样品的电化学行为,例如开路电位(OCP),偏振曲线和电化学阻抗光谱(EIS)。最后,详细讨论了在空化耐腐蚀性耐腐蚀性耐腐蚀性后具有不同微结构的304s的机械性能和腐蚀特性的影响,同时研究了304秒的空化阻力的显微镜机制。结果表明,Surp明显有利于通过引入变形层来保护304s,通过引入变形层,Martensite和奥氏体的转化,钝化膜的形成,晶粒细化和表面硬度以及304s的残余应力。然而,SURP的能量转移不仅用于表面硬化,晶粒细化,滑动带建立,而且形成缺陷,过度的能量转移起着相反的作用。因此,Surp 10次是合适的宿舍,使304s实现最佳的空化阻力。

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