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Annealing strategies for enhancing mechanical properties of additively manufactured 316L stainless steel deposited by cold spray

机译:用于增强冷喷涂沉积的加油316L不锈钢的机械性能的退火策略

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摘要

Cold spray is a solid-state metal deposition and additive manufacturing (AM) technology. The low processing temperatures in cold spraying result in less favorable properties of the deposits as compared to their fusion-based AM counterparts, particularly for materials with high strength such as 316L stainless steel. Therefore, annealing is generally required for the cold sprayed deposits to improve their mechanical properties. In this paper, three different annealing strategies are systematically investigated in order to optimize the microstructure and mechanical properties of cold sprayed 316L stainless steel deposits: air annealing, vacuum annealing, and hot isostatic pressing (HIP), the latter representing a method widely used for densification of components in fusion based metal AM. The results indicate that the three annealing treatments improve the mechanical properties of the cold sprayed 316L stainless steel deposits through grain recrystallization and diffusion at oxide-free interparticle interfaces. Such improvement is less pronounced for the air annealing as a formation of oxide inclusions impedes full inter-particle metallurgical bonding. This effect is suppressed in the vacuum annealing, resulting in a significant improvement in the tensile strength and ductility. Despite the significant improvement in the deposits' density, the HIP results in mechanical properties equivalent to those after vacuum annealing. The experimental results suggest that the strengthening of cold sprayed deposits is mainly dominated by the improved inter-particle bonding and particle grain structure rather than through a reduction of porosity.
机译:冷喷雾是一种固态金属沉积和添加剂制造(AM)技术。与其融合的AM对应物相比,冷喷涂中的低处理温度导致沉积物的较低性质,特别是对于具有高强度,如316L不锈钢的材料。因此,冷喷涂沉积物通常需要退火,以改善其机械性能。在本文中,系统地研究了三种不同的退火策略,以优化冷喷涂316L不锈钢沉积的微观结构和机械性能:空气退火,真空退火和热等静压(臀部),后者代表了广泛用于的方法基于融合的金属am中的组分致密化。结果表明,三种退火处理通过在无氧化物颗粒间接口处改善冷喷涂316L不锈钢沉积的冷喷涂316L不锈钢沉积物的机械性能。由于氧化物夹杂物的形成阻碍了全颗粒冶金结合的空气退火,这种改进不太明显。在真空退火中抑制了这种效果,导致拉伸强度和延展性的显着改善。尽管沉积物密度有显着改善,但髋关节导致在真空退火后的机械性能等同于那些。实验结果表明,加强冷喷涂沉积物主要由改进的颗粒间粘合和颗粒结构而不是通过减少孔隙率。

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