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The effect of ultrasonic nanocrystal surface modification on low temperature nitriding of ultra-high strength steel

机译:超声纳米晶体表面改性对超高强度钢低温氮化的影响

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摘要

In this research, a surface plastic deformation layer was induced on 300M ultra-high strength steel using ultrasonic nanocrystal surface modification (UNSM). The UNSM-treated and control specimens were then nitrided at 450 degrees C for 6 h. After gas nitriding, the microstructure, corrosion and wear resistance of 300M steel with and without UNSM pre-treatment were investigated. After nitriding, the UNSM-treated specimens generated a dense surface nitride layer that was thicker than that of the control specimens. The high defect density and refined lath martensite induced by UNSM were found to accelerate the nitrogen diffusion and efficiency. X-ray diffraction patterns revealed that alpha-Fe phase occupied the largest proportion in the nitriding layer of specimens without UNSM pre-treatment. However due to the higher nitriding efficiency, the main phase of UNSM-treated specimens after nitriding was found to be epsilon-Fe2.3N. Compared with the specimens without pre-treatment, UNSM-treated specimens exhibited higher surface hardness as well as higher corrosion and wear resistance after nitriding.
机译:在该研究中,使用超声纳米晶体表面改性(UNSM)在300m超高强度钢上诱导表面塑性变形层。然后在450℃下氮化未治疗和对照样品6小时。在氮化气体后,研究了300米钢的微观结构,腐蚀和耐磨性,具有和不具有UNS的预处理。氮化后,未处理的样品产生浓稠的表面氮化物层,该氮化物层比对照样品厚。发现由UNSM诱导的高缺陷密度和精制的Lath Martensite加速氮气扩散和效率。 X射线衍射图案显示,α-Fe相占据了标本的氮化层中的最大比例,而没有不具有UNSM的预处理。然而,由于氮化效率较高,发现氮化后未经治疗的标本的主阶段是EPSILON-FE2.3N。与没有预处理的标本相比,未经治疗的标本表现出更高的表面硬度以及氮气后的腐蚀和耐磨性更高。

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