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Comparative study of surface modification techniques through average flank wear in high speed steel tools coated with thin TiN film

机译:薄锡膜涂层高速钢工具平均侧面磨损表面改性技术的比较研究

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摘要

Hard coatings are usually applied to improve high speed steel (HSS) tools performance. However, to achieve this aim, a good adhesion between coating film and substrate is necessary. The coating failure, associated to the lack of adhesion to the substrate, can lead to tool premature wear, reducing its efficiency. The surface modification can improve the coating film adhesion levels by modifying substrates surface roughness, and then, ensuring better anchorage of the deposited layer. In this research two techniques of superficial modification, planar sputtering and chemical polishing, were compared. The sputtering uses plasma application, where cations formed in the reactor collide with samples surface, removing material from it. For chemical polishing, it was used acid and alkaline solutions. After surface treatments, all roughness levels were measured using a roughness tester. The Cathodic Cage Plasma Nitriding (CCPN) technique was used to deposit a TiN film on tools surface. Then, X-ray diffraction, Vickers microhardness and SEM tests were carried out to verify the presence of deposited film, as well as its thickness and mechanical properties, and then, machining tests with SAE 1045 steel where performed, applying the coated tools. Optical microscopy was carried out to track average flank wear up to 0.3 mm, characterizing the end of tool life. It can be observed that all the coated tools obtained an increase in its life, registering the variances according to the different roughness profiles. The best results were verified for chemical polishing with acid solution treatment condition, as it allowed longer machining time with less flank wear.
机译:通常应用硬涂层以改善高速钢(HSS)工具性能。然而,为了实现这种目的,需要在涂​​膜和基板之间具有良好的粘附性。与缺乏对基材的粘附相关的涂层破坏可导致工具早熟,降低其效率。表面改性可以通过改变基板表面粗糙度来改善涂膜粘附水平,然后确保更好的沉积层的锚固。在这项研究中,比较了两种浅表改性,平面溅射和化学抛光的技术。溅射使用等离子体施加,其中在反应器中形成的阳离子与样品表面碰撞,从中除去材料。用于化学抛光,用酸和碱性溶液。在表面处理后,使用粗糙度测试仪测量所有粗糙度水平。将阴极笼等离子体氮化(CCPN)技术用于在工具表面上沉积锡膜。然后,进行X射线衍射,维氏微硬度和SEM测试以验证沉积膜的存在,以及其厚度和机械性能,然后用SAE 1045钢加工测试,在那里进行,涂覆涂层工具。进行光学显微镜,以跟踪平均侧面磨损,高达0.3mm,表征刀具寿命的结束。可以观察到,所有涂覆的工具都获得了其寿命的增加,根据不同的粗糙度轮廓注册差异。用酸性溶液处理条件验证了最佳结果,验证了化学抛光,因为它允许较长的加工时间与较少的侧面磨损。

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