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Synthesis, Characterization and Catalytic Properties of Attapulgite/CeO2 Nanocomposite Films for Decomposition of Rhodamine B

机译:凹凸棒石/ CeO2纳米复合膜的合成,表征及对罗丹明B分解的催化性能

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ATP(attapulgite)/CeO2 nanocomposite films were prepared on the glass substrates via a sol-gel and dip-coating route. The ATP/CeO2 nanocomposite films were characterized by Powder X-ray diffraction (PXRD), scanning electron microscopy (SEM), energy-dispersive spectrometry (EDS), transmission electron microscopy (TEM), atomic force microscopy (AFM) and fourier transform infrared spectroscopy (FT-IR). The results showed that the ATP/CeO2 nanoconnposite films were free from cracks and the nanoparticles were attached onto the surface of attapulgite. The ATP/CeO2 nanocomposite films displayed excellent catalytic activity for decomposition of Rhodamine B. The COD (chemical oxygen demand) removal rate of rhodamine B using ATP/CeO2 nanocomposite films as catalyst reached as high as 94% when the weight ratio of ATP to CeO2 was 2:1.
机译:通过溶胶-凝胶法和浸涂法在玻璃基板上制备ATP(凹凸棒石)/ CeO2纳米复合薄膜。 ATP / CeO2纳米复合薄膜的特征在于粉末X射线衍射(PXRD),扫描电子显微镜(SEM),能量色散光谱(EDS),透射电子显微镜(TEM),原子力显微镜(AFM)和傅立叶变换红外光谱光谱(FT-IR)。结果表明,ATP / CeO2纳米复合薄膜无裂纹,纳米粒子附着在凹凸棒石表面。 ATP / CeO2纳米复合膜对罗丹明B的分解显示出优异的催化活性。当ATP / CeO2纳米复合膜的重量比为ATP时,若以罗丹明B为催化剂,化学需氧量的去除率高达94%。是2:1。

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