Solid-solid synthesis of a hydrophobic vitamin B_(12) having a benzo-18-crown-6 moiety at the C10 position of the corrin ring

Hisashi Shimakoshi; Tetsuo Inaoka; Yoshio Hisaeda

首页> 外文期刊>Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry >Solid-solid synthesis of a hydrophobic vitamin B_(12) having a benzo-18-crown-6 moiety at the C10 position of the corrin ring

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Solid-solid synthesis of a hydrophobic vitamin B_(12) having a benzo-18-crown-6 moiety at the C10 position of the corrin ring

机译：固-固合成疏水蛋白B_（12），该蛋白在corrin环的C10位置具有苯并18-冠-6部分

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摘要

A new hydrophobic vitamin B_(12) having a benzo-18-crown-6 moiety at the C-10 position of the corrin ring was synthesized by solid-state condensation reaction. The proton NMR titration study in acetonitrile exhibits a potassium ion binding behavior of the hydrophobic vitamin B_(12) at the benzo-18-crown-6 moiety.

机译：通过固相缩合反应合成了一种新的疏水性维生素B_（12），该维生素B_（12）在corrin环的C-10位具有苯并18-冠-6部分。乙腈中的质子NMR滴定研究显示了疏水性维生素B_（12）在苯并18-冠-6部分的钾离子结合行为。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2003年第34期|共4页
作者
Hisashi Shimakoshi; Tetsuo Inaoka; Yoshio Hisaeda;
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hydrophobic vitamin B_(12); benzo-18-crown-6; solid-state reaction; potassium ion binding;

机译：疏水性维生素B_（12）;苯并18-冠-6;固相反应;钾离子结合;

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1. Solid-solid synthesis of a hydrophobic vitamin B_(12) having a benzo-18-crown-6 moiety at the C10 position of the corrin ring [J] . Hisashi Shimakoshi, Tetsuo Inaoka, Yoshio Hisaeda Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2003,第34期

机译：固-固合成疏水蛋白B_（12），该蛋白在corrin环的C10位置具有苯并18-冠-6部分
2. Hydrophobic vitamin B_(12). Part 18. Preparation of a sol-gel modified electrode trapped with a vitamin B_(12) derivative and its photoelectrochemical reactivity [J] . Hisashi Shimakoshi, Aki Nakazato, Mami Tokunaga, Dalton transactions: An international journal of inorganic chemistry . 2003,第11期

机译：疏水性维生素B_（12）。第18部分。捕获有维生素B_（12）衍生物的溶胶-凝胶修饰的电极的制备及其光电化学反应性
3. Electroorganic syntheses of macrocyclic lactones mediated by vitamin B_(12) model complexes Part 17.Hydrophobic vitamin B_(12) [J] . Hisashi Shimakoshi, Aki Nakazato, Takashi Hayashi Journal of Electroanalytical Chemistry: An International Journal Devoted to All Aspects of Electrode Kinetics, Interfacial Structure, Properties of Electrolytes, Colloid and Biological Electrochemistry . 2001,第1a2期

机译：维生素B_（12）模型复合物介导的大环内酯的有机合成第17部分疏水性维生素B_（12）
4. Vitamin B_(12) in Muscle Foods. Comparison of a Microbiological Assay and a Fully Automated Chemiluminescence System for the Determination of Vitamin B_(12) in Fresh and Processed Meat. [C] . Saccani G. ICoMST 2011;International conference of meat science and technology . 2012

机译：肌肉食品中的维生素B_（12）。微生物测定和全自动化学发光系统测定鲜肉和加工肉中维生素B_（12）的比较。
5. Studies of the last step of de novo corrin ring biosynthesis and the nucleotide loop assembly pathway of coenzyme B(12) synthesis [D] . Zayas Aponte, Carmen Loyda. 2007

机译：研究De Novo Corrin环生物合成的最后一步和辅酶B（12）合成的核苷酸环组装路径
6. Biosynthesis of vitamin B12: nature of the volatile fragment generated during formation of the corrin ring system. [O] . L Mombelli, C Nussbaumer, H Weber, 1981

机译：维生素B12的生物合成：在柯林环系统形成过程中产生的挥发性片段的性质。
7. Biosynthesis of vitamin B-12 in anaerobic bacteria. Experiments with Eubacterium limosum on the origin of the amide groups of the corrin ring and of N-3 of the 5,6-dimethylbenzimidazole part [O] . Joachim R. A. VOGT, Paul RENZ 1988

机译：厌氧细菌维生素B-12的生物合成。用细菌材料对酰胺基团的起源和5,6-二甲基苯并咪唑部分的酰胺基团的起源的实验
8. Synthesis of Potential Metaboliters in the 1,2,3,4, and 5,6,7,8 Benzo Ring Positions of the Polycyclic Aromatic Hydrocarbon Benzo(G)Chrysene [R] . Utermoehlen, C. M. 1986

机译：在多环芳烃（G）Chrysene的1,2,3,4和5,6,7,8苯并环位置合成潜在的代谢物

Solid-solid synthesis of a hydrophobic vitamin B_(12) having a benzo-18-crown-6 moiety at the C10 position of the corrin ring

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