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Synthesis, FTIR, UV-Vis and Photoluminescence characterizations of triethanolamine passivated CdO nanostructures

机译:三乙醇胺钝化的CdO纳米结构的合成,FTIR,UV-Vis和光致发光特性

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In this study, triethanolamine (TEOA) capped CdO nanostructures had been synthesized by wet chemical method annealed at 648 K were reported. The structural, morphological and optical properties of the samples were studied by X-ray diffraction (XRD), Field emission scanning electron microscopy (FESEM) with energy dispersive spectra (EDS) analysis, Fourier transform infrared (FTIR) spectroscopy, UV-Vis spectroscopy and Photoluminescence (PL) techniques. The XRD spectrum showed that all the samples were cubic in structure. The presence of functional groups and chemical bonding had been confirmed by FTIR. UV-Vis measurements showed decreased band gap energy for TEOA capped CdO, when compared with uncapped CdO. The PL spectra of the CdO systems showed the red emission. (C) 2015 Elsevier B.V. All rights reserved.
机译:在这项研究中,报道了通过湿化学法在648 K退火的条件下合成的三乙醇胺(TEOA)封端的CdO纳米结构。通过X射线衍射(XRD),具有能量色散光谱(EDS)分析的场发射扫描电子显微镜(FESEM),傅里叶变换红外(FTIR)光谱,UV-Vis光谱研究了样品的结构,形态和光学性质和光致发光(PL)技术。 XRD谱图表明,所有样品均为立方结构。 FTIR已证实官能团和化学键的存在。 UV-Vis测量显示,与未封端的CdO相比,TEOA封端的CdO的带隙能量降低。 CdO系统的PL光谱显示红色发射。 (C)2015 Elsevier B.V.保留所有权利。

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