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Preparation of c-axis textured SiC ceramics by a strong magnetic field of 6 T assisted gel-casting process

机译:6 T强磁场辅助凝胶铸造法制备c轴织构SiC陶瓷

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C-axis textured SiC ceramics were prepared by a strong magnetic field of 6 T assisted gel-casting and subsequent pressureless sintering. The optimal suspension parameters for gel-casting were determined by analyzing the influences of pH value and dispersant content on the stability and dispersibility of suspensions. The effect of sintering conditions on the texture development and properties of SiC ceramics was discussed. It was found that the increasing sintering temperature or holding time promoted the densification process of SiC ceramics. The c-axis of SiC grain was aligned parallel to the magnetic field by applying a strong magnetic field of 6 T. The degree of texture of SiC ceramics showed a slightly increasing trend with the increase of sintering temperature or holding time. When the samples were sintered at 1950 degrees C for 4 h or 6 h, the large elongated grains were formed in the samples, leading to the extremely evident anisotropic microstructure on different planes. Textured SiC ceramics exhibited the anisotropic bending strength. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
机译:通过6 T辅助凝胶浇铸的强磁场以及随后的无压烧结来制备C轴纹理SiC陶瓷。通过分析pH值和分散剂含量对悬浮液稳定性和分散性的影响,确定了凝胶浇铸的最佳悬浮液参数。讨论了烧结条件对SiC陶瓷织构发展和性能的影响。发现增加的烧结温度或保持时间促进了SiC陶瓷的致密化过程。通过施加6 T的强磁场,使SiC晶粒的c轴平行于磁场对齐。随着烧结温度或保持时间的增加,SiC陶瓷的织构度呈略微增加的趋势。当样品在1950摄氏度下烧结4小时或6小时时,在样品中形成了大的细长晶粒,从而导致在不同平面上具有极其明显的各向异性微观结构。碳化SiC陶瓷具有各向异性的弯曲强度。 (C)2016 Elsevier Ltd和Techna Group S.r.l.版权所有。

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