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Characterization of activated carbon prepared from chlorella-based algal residue

机译:由小球藻基藻渣制备的活性炭的表征

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摘要

The chlorella-based microalgal residue (AR) was tested as a novel precursor for preparing activated carbons. A combined carbonization-activation process with flowing N-2 and CO2 gases was used to prepare the carbon materials at the activation temperatures of 800-1000 degrees C and the residence times of 0-30 min in this work. The elemental contents, pore properties and scanning electron microscopy (SEM) observations of the resulting activated carbons have been performed. The results showed that activation temperature may be the most important parameter for determining their pore properties. The maximal Brunauer-Emmett-Teller (BET) surface area and total pore volume of the resulting activated carbon, which was produced at the activation temperature of 950 degrees C with the residence time of 30 min, were 840 m(2)/g and 0.46 cm(3)/g, respectively. More interestingly, the resulting activated carbons have significant nitrogen contents of 3.6-9.6 wt%, which make them lower carbon contents (i.e., 54.6-68.4 wt%) than those of commercial activated carbons. (C) 2014 Elsevier Ltd. All rights reserved.
机译:基于小球藻的微藻残留物(AR)作为制备活性炭的新型前体进行了测试。在这项工作中,使用流动的N-2和CO2气体的联合碳化活化过程来制备碳材料,其活化温度为800-1000摄氏度,停留时间为0-30分钟。已经进行了所得活性炭的元素含量,孔隙性质和扫描电子显微镜(SEM)观察。结果表明,活化温度可能是确定其孔隙性质的最重要参数。在950℃的活化温度和30分钟的停留时间下产生的活性炭的最大Brunauer-Emmett-Teller(BET)表面积和总孔体积为840 m(2)/ g,分别为0.46 cm(3)/ g。更有趣的是,所得的活性炭具有显着的氮含量为3.6-9.6wt%,这使得它们的碳含量低于市售活性炭的碳含量(即54.6-68.4wt%)。 (C)2014 Elsevier Ltd.保留所有权利。

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