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首页> 外文期刊>Journal of Thermoplastic Composite Materials >Preparation and characterization of thermoplastic acryIate pressure-sensitive adhesiveickel/multiwalled carbon nanotubes
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Preparation and characterization of thermoplastic acryIate pressure-sensitive adhesiveickel/multiwalled carbon nanotubes

机译:热塑性丙烯酸酯压敏胶/镍/多壁碳纳米管的制备与表征

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摘要

In this work, a novel polymer magnetic composite based on thermoplastic acrylate pressure-sensitive adhesive (acrylate PSA) filled with the nickel plating multiwall carbon nanotubes (Ni/MWNTs) were prepared using Ni/MWNTs obtained by electroless plating method. Then their morphology and properties were characterized by transmission electron microscope, scanning electron microscope (SEM), X-ray diffraction (XRD), vibrating sample magnetometer (VSM) and so on. Both SEM and XRD indicate that a large number of nickel particles are homogenously coated on the surface of MWNTs. SEM reveals that the Ni/MWNTs are homogeneously dispersed in thermoplastic acrylate PSA. The VSM show that the saturation magnetization (M_s) of the Ni/MWNTs is 92.0 emu/g and the increase in the Ni/MWNTs content could enhance the M_s of the thermoplastic acrylate PSA/Ni/MWNTs composites and decrease their coercivity (H_c). When the content of Ni/MWNTs is 10.0 wt%, the magnetic and mechanical properties of the thermoplastic acrylate PSA/Ni/MWNTs composites are optimum.
机译:在这项工作中,使用通过化学镀方法获得的Ni / MWNTs,制备了一种新型的基于热塑性丙烯酸酯压敏粘合剂(丙烯酸酯PSA)的聚合物磁性复合材料,其中填充了镀镍的多壁碳纳米管(Ni / MWNTs)。然后用透射电子显微镜,扫描电子显微镜(SEM),X射线衍射(XRD),振动样品磁力计(VSM)等对它们的形貌和性能进行了表征。 SEM和XRD都表明大量镍颗粒均匀地涂覆在MWNTs的表面上。 SEM显示,Ni / MWNTs均匀分散在热塑性丙烯酸酯PSA中。 VSM结果表明,Ni / MWNTs的饱和磁化强度(M_s)为92.0 emu / g,Ni / MWNTs含量的增加可以提高热塑性丙烯酸酯PSA / Ni / MWNTs复合材料的M_s并降低其矫顽力(H_c) 。当Ni / MWNTs的含量为10.0wt%时,热塑性丙烯酸酯PSA / Ni / MWNTs复合材料的磁性和机械性能最佳。

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