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Sliding Wear Response of Nanostructured YSZ Suspension Plasma-Sprayed Coating

机译:纳米结构YSZ悬浮等离子喷涂涂层的滑动磨损响应

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摘要

Nanostructured yttria-stabilized zirconia coatings for applications in high-temperature environments can be deposited by suspension plasma spraying (SPS) techniques. The present research has been conducted in order to study the sliding wear response of a SPS ZrO2-8% mol. Y2O3 coating (75 mu m in thickness) deposited onto a Haynes 230 substrate, using pin-on-disc tests. Some of the coated samples were subsequently heat-treated for 1 h at 300 and 600 A degrees C. Samples characterization prior and after the wear tests was carried out by SEM, EDS, XRD and optical profilometry techniques. Instrumented indentation was employed to determine elastic modulus and hardness. The results have shown that the as-sprayed and heat-treated samples experienced severe wear (10(-13) m(3)/Nm) and the worst wear performance corresponded to the sample heat treated at 600 A degrees C. Such a behavior could be related to both the structural changes that took place during heat treatment and the nature and level of the residual stresses in the coatings. In general, the morphologies of the wear tracks observed by SEM have shown a smoothing of the surface, brittle fracture, smearing and grain pull-out.
机译:可通过悬浮等离子喷涂(SPS)技术沉积用于高温环境的纳米结构的氧化钇稳定的氧化锆涂层。为了研究SPS ZrO2-8%mol的滑动磨损响应,进行了本研究。使用针对盘测试,将Y2O3涂层(厚度为75μm)沉积在Haynes 230基板上。随后将一些涂覆的样品在300和600 A的温度下热处理1小时。通过SEM,EDS,XRD和光学轮廓测量技术对磨损测试前后的样品进行表征。使用仪器压痕确定弹性模量和硬度。结果表明,喷涂和热处理后的样品经历了严重磨损(10(-13)m(3)/ Nm),最差的磨损性能对应于在600 A摄氏度下热处理的样品。可能与热处理过程中发生的结构变化以及涂层中残余应力的性质和水平有关。通常,通过SEM观察到的磨损轨迹的形态显示出表面的平滑,脆性断裂,涂抹和晶粒拉出。

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