The effect of zirconia sintering temperature on flexural strength, grain size, and contrast ratio

摘要

Objective: This study investigated the effect of sintering temperatures on flexural strength, contrast ratio, and grain size of zirconia. Materials and Methods: Zirconia specimens (Ceramill ZI, Amann Girrbach) were prepared in partially sintered state. Subsequently, the specimens were randomly divided into nine groups and sintered with different final sintering temperatures: 1,300°C, 1,350°C, 1,400°C, 1,450°C, 1,500°C, 1,550°C, 1,600°C, 1,650°C, or 1,700°C with 120 min holding time. Three-point flexural strength (N = 198; n = 22 per group) was measured according to ISO 6872: 2008. The contrast ratio (N = 90; n = 10 per group) was measured according to ISO 2471: 2008. Grain sizes and microstructure of different groups were investigated (N = 9, n = 1 per group) with scanning electron microscope. Data were analyzed using one-way ANOVA with Scheffé test and Weibull statistics (p<0.05). Pearson correlation coefficient was calculated between either flexural strength or contrast ratio and sintering temperatures. Results: The highest flexural strength was observed in groups sintered between 1,400°C and 1,550°C. The highest Weibull moduli were obtained for zirconia sintered at 1,400°C and the lowest at 1,700°C. The contrast ratio and the grain size were higher with the higher sintering temperature. The microstructure of the specimens sintered above 1,650°C exhibited defects. Sintering temperatures showed a significant negative correlation with both the flexural strength (r = -0. 313, p<0. 001) and the contrast ratio values (r = -0. 96, p<0. 001). Conclusions: The results of this study showed that the increase in sintering temperature increased the contrast ratio, but led to a negative impact on the flexural strength. Clinical Relevance: Considering the flexural strength values and Weibull moduli, the sintering temperature for the zirconia tested in this study should not exceed 1,550°C.