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首页> 外文期刊>Journal of thermal analysis and calorimetry >Characterization of sugar palm (Arenga pinnata) fibres Tensile and thermal properties
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Characterization of sugar palm (Arenga pinnata) fibres Tensile and thermal properties

机译:糖棕(Arenga pinnata)纤维的表征拉伸和热性能

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摘要

The aim of this study was to characterize tensile and thermal properties of sugar palm (Arenga pinnata) fibres obtained from different heights (1, 3, 5, 7, 9, 11, 13, and 15 m) of sugar palm tree. This study has confirmed that in a mature sugar palm tree, degradation was occurred and altered the properties of its fibre. Fibres obtained at the area of live (green) palm frond were found to have a better tensile properties as a result of its optimum chemical composition especially cellulose, hemicelluloses and lignin. For the fibre obtained from the upper part of sugar palm tree, it shows slightly decreasing trend in tensile properties compared to mature fibres. It is due to the fibres are juvenile where their cell walls are progressively built up thus give slightly lower properties than matured fibres. For the fibre obtained from the area of dead palm frond, the fibres are considered to be degraded biologically. It is believed that polymeric chains in microfibrils were broken and their cellulose content was decreased which demonstrated inferior properties (tensile strength, modulus, elongation at break and toughness). The use of such fibre for application as reinforcing fibre in composite is not recommended since the strength of the fibre and composite will be reduced. There were four phases of decomposition of the fibres where the sequence of decomposition started with decomposition of moisture, followed by hemicelluloses, then cellulose and next is lignin while the ash was the last component left. The thermal degradation of these components were found in ranges of 45-123, 210-300, 300-400, 160-900 and 1723°C, respectively. Thermogravimetric analysis and derivative thermogravimetric analysis curves showed that the fibre of 1 m showed higher thermal stability than the fibres of 3-15 m. The different thermal stability for each fibre was due to different chemical compositions especially when the fibre containing high ash content which result in higher thermal stability.
机译:这项研究的目的是表征从不同高度(1、3、5、7、9、11、13和15 m)的糖棕树获得的糖棕(Arenga pinnata)纤维的拉伸和热性能。这项研究已经证实,在成熟的sugar榔树中,会发生降解并改变其纤维的特性。由于其最佳的化学组成,特别是纤维素,半纤维素和木质素,发现在活(绿色)棕榈叶地区获得的纤维具有更好的拉伸性能。对于从糖棕树上部获得的纤维,与成熟纤维相比,它的拉伸性能略有下降。这是由于纤维是幼小的,其细胞壁逐渐积聚,因此其性能比成熟纤维略低。对于从死棕榈叶区域获得的纤维,认为该纤维在生物学上是降解的。据信,微纤维中的聚合物链断裂并且其纤维素含量降低,这表明性能较差(抗张强度,模量,断裂伸长率和韧性)。不推荐使用这种纤维作为复合材料中的增强纤维,因为这样会降低纤维和复合材料的强度。纤维有四个分解阶段,分解顺序从水分分解开始,然后是半纤维素,然后是纤维素,其次是木质素,而灰分是剩下的最后一个成分。发现这些组分的热降解分别在45-123、210-300、300-400、160-900和1723°C的范围内。热重分析和微分热重分析曲线表明,1 m的纤维比3-15 m的纤维具有更高的热稳定性。每种纤维的不同热稳定性是由于化学成分不同而引起的,尤其是当纤维中灰分含量较高时,会导致较高的热稳定性。

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