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Modification of Type Analysis for Heavy Oil by Downsizing of JPI Standard (JPI-5S-22-83)

机译:通过精简JPI标准(JPI-5S-22-83)修改重油类型分析

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摘要

A modified type analysis method (DS method) for heavy oil was conducted using a Liebig condenser as a column, which scale was about 1/4 as prescribed in the JPI standard (JPI-5S-22-83). Two kinds of maltenes (pentane soluble fractions), those from Middle East vacuum residue (ME) and Cold Lake oil sand bitumen atmospheric residue (CL), were separated into saturates, aromatics and resins by JPI and DS methods. The repeatability errors for the recoveries of respective saturates, aromatics and resins were within 2 wt% on each experiments. The recoveries of corresponding fractions between both methods were well agreed to each other, and also the results of elemental analysis. Those results indicate that the DS method is available as an alternative method to the JPI standard.
机译:使用Liebig冷凝器作为色谱柱,对重油进行了改进的类型分析方法(DS方法),其规模约为JPI标准(JPI-5S-22-83)规定的1/4。通过JPI和DS方法将来自中东真空渣油(ME)和冷湖油砂沥青常压渣油(CL)的两种麦芽糖(戊烷可溶级分)分为饱和物,芳烃和树脂。在每个实验中,各饱和物,芳烃和树脂的回收率的重复性误差均在2 wt%之内。两种方法之间相应馏分的回收率彼此一致,而且元素分析的结果也很一致。这些结果表明,DS方法可作为JPI标准的替代方法。

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