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Experimental study of the break-up of starch suspension droplets in step-up shear flow

机译:逐步剪切流动中淀粉悬浮液液滴破碎的实验研究

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The deformation and break-up of a droplet of suspension of swollen-in-water starch granules placed in an immiscible fluid, silicon oil, are investigated. The study was carried out on a physically modified waxy maize starch suspension with a theoretical granule volume fraction of 100%. Granules were swollen to their maximum; they were highly deformable. Measurements were carried out using a counter rotating shear cell. The starch suspension was shear thinning above a yield stress of about 90-100 Pa showing elasticity (first normal stress difference) above 300 Pa. The rheo-optical experiments were carried out by stepping up the stress from zero to a constant value and deformation of suspension droplets of various sizes was observed with time. Critical break-up capillary numbers Ca~* were calculated and correlated with droplet-to-matrix viscosity ratio p. At low p values Ca~* were found to be smaller or close to those determined for Newtonian fluids. No break-up was observed for viscosity ratios above 0.1, a limit that is roughly 40 times lower than that for the Newtonian fluids. This result was assumed to be due to the fact that internal stress in the droplet is lower than the mean one applied, because of inter-particle interactions and friction, thus shifting suspension from low to extremely high viscosity fluid if applied stress is close to the yield transition.
机译:研究了混溶在硅油中的水溶胀淀粉颗粒悬浮液液滴的变形和破裂。该研究是在理论上颗粒体积分数为100%的物理改性蜡质玉米淀粉悬浮液上进行的。颗粒膨胀到最大。它们极易变形。使用反向旋转剪切池进行测量。淀粉悬浮液在高于90-100 Pa的屈服应力下被剪切稀化,显示出300 Pa以上的弹性(第一法向应力差)。流变光学实验是通过将应力从零增加到恒定值并变形而进行的。随时间观察到各种尺寸的悬浮液滴。计算了临界破裂毛细管数Ca〜*,并将其与液滴与基质的粘度比p相关联。在低p值时,发现Ca〜*小于或接近为牛顿流体确定的值。对于高于0.1的粘度比,没有观察到破裂,该极限大约比牛顿流体的极限低40倍。假定该结果是由于以下事实:由于颗粒间的相互作用和摩擦,液滴中的内部应力低于施加的平均应力,因此,如果施加的应力接近于液滴,则悬浮液会从低粘度流体变为极高粘度的流体。产量过渡。

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