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Temperature Distribution in a Microwave Heated Gas Chromatographic Packed Column

机译:微波加热气相色谱填充柱中的温度分布

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To understand how to use microwaves more efficiently to enhance chromatographic separation, we have to understand how the material with which they interact is affected. This is addressed by formulating and solving the energy equation to predict the temperature distribution in the chromatographic column. This issue is addressed in this article by modeling the microwave heated packed column to obtain a temperature difference between the gas and solid pellets. The effect of some parameters on the solid-gas temperature difference in the packed chromatographic column is investigated. Calculated gas velocity and temperature difference reflect their sensitivity to inlet gas velocity, solid particle diameter, and electric field. The used numerical procedure offers an efficient tool to evaluate whether the solid particles can be heated to a higher temperature than the gas in the chromatographic column. Because of the high solid pellet temperature, the separation process will be greatly enhanced in the vicinity of the solid particles.
机译:为了了解如何更有效地使用微波来增强色谱分离效果,我们必须了解与之相互作用的材料是如何受到影响的。这可以通过公式化和求解能量方程来预测色谱柱中的温度分布来解决。在本文中,通过对微波加热的填充塔进行建模以获得气体颗粒和固体颗粒之间的温差来解决此问题。研究了一些参数对填充色谱柱中固相气温差的影响。计算出的气体速度和温度差反映了它们对入口气体速度,固体颗粒直径和电场的敏感性。所使用的数值程序提供了一种有效的工具,可以评估固体颗粒是否可以加热到比色谱柱中的气体更高的温度。由于固体颗粒温度高,固体颗粒附近的分离过程将大大增强。

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