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Synthesis and characterizations of graphene-copper nanocomposites and their antifriction application

机译:石墨烯-铜纳米复合材料的合成,表征及其减摩应用

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摘要

In this work, a facile one-pot reduction method was used to prepare graphene-copper nanocomposites using graphite oxide and copper sulfate. The nanocomposites were characterized by transmission electron microscope, X-ray diffraction, Raman spectrum, thermal gravimetric analysis, UV-vis analysis and Fourier transform infrared spectrum. It was found that the as-synthesized graphene sheets have few layers and less defects with oxygen functional group on it. The copper nanoparticles with an average diameter of 20 nm were uniformly deposited on the graphene sheets. The aggregation of the copper nanoparticles was effectively prevented. The nanocomposites can evenly disperse in base oil. The antifriction performance of the base oil added with GNS-Cu was firstly investigated. It was found that the GNS-Cu nanocomposites as additive in proper ratio showed better antifriction properties with an improvement of the load-carrying capacity by 50%.
机译:在这项工作中,一种简便的一锅还原法被用于使用氧化石墨和硫酸铜制备石墨烯-铜纳米复合材料。通过透射电子显微镜,X射线衍射,拉曼光谱,热重分析,UV-vis分析和傅立叶变换红外光谱对纳米复合材料进行表征。发现合成后的石墨烯片几乎没有层并且带有氧官能团的缺陷较少。将平均直径为20nm的铜纳米颗粒均匀地沉积在石墨烯片上。有效地防止了铜纳米颗粒的聚集。纳米复合材料可以均匀地分散在基础油中。首先研究了添加GNS-Cu的基础油的减摩性能。发现以适当比例的GNS-Cu纳米复合材料作为添加剂显示出更好的减摩性能,其承载能力提高了50%。

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