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Characteristics of nano-sized perovskite structured LaSrMn derived from hydrothermally synthesized amorphous LaSrMn oxide powder

机译:水热合成非晶态LaSrMn氧化物粉末衍生的纳米钙钛矿结构LaSrMn的特征

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摘要

Nano-sized and spherical shaped LaSrMn oxide particle was synthesized by thermal treatment at 900 °C for 3 h after hydrothermally treatment at 200 °C for 8 h, and characterized to be applied as a cathode material in solid oxide fuel cells. A spherical LSM nano-particle with sizes ranging from 100 to 120 ,nm was shown in SEM image and particle size distribution. The pellets of five types composed of χ-wt% LSM synthesized and commercial γ-wt% YSZ were manufactured and pre-sintered. Their ionic conductivities were enhanced responding to LSM concentrations, and it was the highest in 8LSM:2YSZ showing 74.0 S cm~(-1).
机译:纳米球形LaSrMn氧化物颗粒是在200°C水热处理8 h后,在900°C热处理3 h​​合成得到的,并被表征为固体氧化物燃料电池的正极材料。在SEM图像和粒度分布中显示了球形LSM纳米颗粒,其尺寸范围为100至120nm。制造并预烧结了由合成的χ-wt%LSM和商品γ-wt%YSZ组成的五种颗粒。它们的离子电导率随LSM浓度的增加而增强,在8LSM:2YSZ中最高,达到74.0 S cm〜(-1)。

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