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Fabrication of TiB2 nanoparticulates-reinforced aluminum matrix composites by powder metallurgy route

机译:粉末冶金法制备TiB2纳米颗粒增强铝基复合材料

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摘要

Al/TiB2 nanocomposites were fabricated via powder metallurgy route through a primarily cold isostatic pressing of aluminum powder containing 1.5, 2.5, 3.5, 5, and 10 Vol.% of TiB2 nanoparticles and subsequent sintering at two temperatures of 650? and 680?. Density, phase analysis, microstructure, and compressive strength of the samples were then characterized. Results indicated that with increasing the content of the second phase (TiB2), the amount of structural deteriorations like porosity and crack increases as a result of poorer distribution of ceramic nanoparticles, agglomeration, and retarded sintering. However, the compressive strength of nanocomposites tends to enhance with addition and increasing the amount of reinforcement phase (TiB2). Improvement in the compressive strength of composites is a result of activation of strengthening mechanisms such as formation and pile-up of dislocations. The trend of the compressive strength decreases after reaching a maximum amount for Al-2.5TiB(2), in 680?. Generally, samples with moderate amounts of TiB2 (2.5-5 Vol.%) have shown better microstructural and mechanical characteristics due to efficient impact of strengthening mechanisms with lower negative effects of destructive factors like porosity and agglomeration.
机译:Al / TiB2纳米复合材料是通过粉末冶金工艺制造的,首先对含有1.5、2.5、3.5、5和10 Vol。%TiB2纳米颗粒的铝粉进行冷等静压,然后在两个温度650°C下烧结。和680?然后表征样品的密度,相分析,微观结构和抗压强度。结果表明,随着第二相(TiB2)含量的增加,由于陶瓷纳米颗粒的分布较差,团聚和烧结延迟,结构变质的程度(例如孔隙率和裂纹)增加了。然而,纳米复合材料的抗压强度趋于随着添加和增强相(TiB2)的量的增加而增强。复合材料抗压强度的提高是激活强化机制(如位错的形成和堆积)的结果。 Al-2.5TiB(2)在680?中达到最大值后,抗压强度的趋势降低。通常,由于增强机制的有效影响以及较低的破坏性因素(如孔隙度和团聚)负面影响,中等含量的TiB2(2.5-5 Vol。%)样品显示出更好的微观结构和机械特性。

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