X-ray crystal structures of ethoxycarbonyl-, diethyl-2-triphenyl-λ~5 phosphoranylidene- N -phenylimide derivatives

Arsanious Mona H.N.

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X-ray crystal structures of ethoxycarbonyl-, diethyl-2-triphenyl-λ~5 phosphoranylidene- N -phenylimide derivatives

机译：乙氧基羰基-，二乙基-2-三苯基-λ〜5亚磷叉基-N-苯基酰亚胺衍生物的X射线晶体结构

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Phenylisothiocyanate reacts with ethyltriphenylphosphanylideneacetate at room temperature to yield 2-(ethoxycarbonyl)-2-(triphenyl- λ 5 -phosphanylidene)-N' -phenylethane thioimidic acid and diethyl-2-(triphenyl- λ 5 -phosphanylidene)-3-(phenylimino)pentanedioate. The formation of phosphoranes are explained according to mechanism of the Wittig type reaction. The X-ray analysis structures of phosphorane adducts were studied.

机译：苯基异硫氰酸酯在室温下与三苯基膦基亚乙基乙酸乙酯反应生成2-（乙氧基羰基）-2-（三苯基-λ5-膦基亚烷基）-N'-苯基乙烷硫代亚氨酸酸和二乙基-2-（三苯基-λ5-膦基亚基）-3-（苯基亚氨基））戊二酸根据维蒂希型反应的机理解释了膦烷的形成。研究了磷烷加合物的X射线分析结构。

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《Journal of chemical research: reviews and research papers from all branches of chemistry》 |2010年第12期|共4页
作者
Arsanious Mona H.N.;
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正文语种 eng
中图分类化学;
关键词
PHENYLISOTHIOCYANATE; PHOSPHONIUM YLIDE; PHOSPHANYLIDENE COMPOUNDS;

机译：苯基异硫氰酸酯;磷化膦;亚苯基化合物;

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1. X-ray crystal structures of ethoxycarbonyl-, diethyl-2-triphenyl-λ~5 phosphoranylidene- N -phenylimide derivatives [J] . Arsanious Mona H.N. Journal of chemical research: reviews and research papers from all branches of chemistry . 2010,第12期

机译：乙氧基羰基-，二乙基-2-三苯基-λ〜5亚磷叉基-N-苯基酰亚胺衍生物的X射线晶体结构
2. Crystal and molecular structures of three 2-substituted 4-methyloxan-4-ol derivatives studied by X-ray crystallography and by PM6 calculations [J] . Zukerman-Schpector J, Dos Santos AA, Macedo A, Zeitschrift fur Kristallographie: International Journal for Structural, Physical, and Chemical Aspects of Crystalline Materials . 2008,第7期

机译：通过X射线晶体学和PM6计算研究了三种2-取代的4-甲基-氧杂-4-醇衍生物的晶体和分子结构
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机译：HOTeF5和HN（sO2CF3）2的甲基锡（IV）衍生物：（CH3）2snC1（OTeF5）和（CH3）3sn（H2O）2N（sO2CF3）2的溶液多核磁共振研究和X射线晶体结构

X-ray crystal structures of ethoxycarbonyl-, diethyl-2-triphenyl-λ~5 phosphoranylidene- N -phenylimide derivatives

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