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Effects of atmospheric pressure helium/air plasma treatment on adhesion and mechanical properties of aramid fibers

机译:大气压氦/空气等离子体处理对芳纶纤维附着力和力学性能的影响

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摘要

In order to investigate the effect of atmospheric pressure plasmas on adhesion between aramid fibers and epoxy, aramid fibers were treated with atmospheric pressure helium/air for 15, 30 and 60 s on a capacitively-coupled device at a frequency of 5.0 kHz and He outlet pressure of 3.43 kPa. SEM analysis at 10 000 X magnification showed no significant surface morphological change resulted from the plasma treatments. XPS analysis showed a decrease in carbon content and an increase in oxygen content. Deconvolution analysis of C1s, N1s and O1s peaks showed an increase in surface hydroxyl groups that can interact with epoxy resin. The microbond test showed that the plasma treatment for 60 s increased interfacial shear strength by 109% over that of the control (untreated). The atmospheric pressure plasma increased single fiber tensile strength by 16-26%.
机译:为了研究大气压等离子体对芳族聚酰胺纤维与环氧树脂之间的粘附力的影响,在电容耦合设备上以5.0 kHz的频率和氦气出口对大气压下的芳族聚酰胺纤维进行了大气压氦/空气处理15、30和60 s压力为3.43 kPa。放大倍数为10000 X的SEM分析表明,等离子体处理不会导致明显的表面形态变化。 XPS分析显示碳含量降低,氧含量提高。对C1s,N1s和O1s峰进行反卷积分析表明,可以与环氧树脂相互作用的表面羟基增加。微键测试表明,与对照(未处理)相比,等离子处理60 s可使界面剪切强度提高109%。大气压等离子体使单纤维的抗张强度提高了16%至26%。

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