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首页> 外文期刊>Journal of Applied Polymer Science >Study of Nanocrystalline TiO_2 Prepared with Raw and Modified Gelatin Dispersants
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Study of Nanocrystalline TiO_2 Prepared with Raw and Modified Gelatin Dispersants

机译:生胶和改性明胶分散剂制备纳米TiO_2的研究

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摘要

Nanocrystalline TiO_2 was prepared by the sol-gel method, and raw gelatin and its modified samples crosslinked with formaldehyde acted as dispersers in this method. Transmission electron microscope and X-ray diffractometer measurements showed, suing modified gelatin samples, the prepared TiO_2 nanocrystals have smaller particle size and more homogeneous particle distribution at the same calcining temperature. Following Fourier transform IR spectroscope analysis, the dispersion mechanism is considered to be through the bonding of TiO(NO_3)_2.H_2O with the peptide chains of gelatin by a hydrogen bond.
机译:采用溶胶-凝胶法制备了纳米TiO_2,并以明胶及其与甲醛交联的改性样品为分散剂。透射电子显微镜和X射线衍射仪的测量结果表明,使用改性明胶样品,在相同的煅烧温度下,制备的TiO_2纳米晶体具有较小的粒径和较均匀的颗粒分布。通过傅里叶变换红外光谱仪分析,认为分散机理是通过氢键将TiO(NO_3)_2.H_2O与明胶的肽链结合。

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