首页> 外文期刊>Zeitschrift fur Physikalische Chemie: International Journal of Research in Physical Chemistry and Chemical Physics >Preparation and Characterization of Al2O3 Doped TiO2 Nanocomposites Prepared from Simple Sol-Gel Method
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Preparation and Characterization of Al2O3 Doped TiO2 Nanocomposites Prepared from Simple Sol-Gel Method

机译:简单溶胶凝胶法制备Al2O3掺杂的TiO2纳米复合材料的制备与表征

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Al2O3 doped TiO2 samples were prepared by the simple sol-gel method. The prepared samples were annealed at 400 degrees C for 1 h in an open air atmosphere. The dielectric properties, AC electrical conductivity (sigma(ac)), dielectric constant (epsilon'), dielectric loss (epsilon '') and the loss tangent (tan delta) of the prepared Al2O3 doped TiO2 nanocomposites were studied under a wide frequency and temperature range. The dielectric loss values of the prepared samples were measured at 50 Hz and 5 MHz and the values were found to be in the range of 0.11-1.73 at 40 degrees C and 0.13-4.39 at 100 degrees C. The microstructures of the prepared samples were also studied using high-resolution transmission electron microscopy (HRTEM) analysis.
机译:采用简单的溶胶-凝胶法制备了掺杂Al2O3的TiO2样品。将制备的样品在露天气氛中在400摄氏度下退火1小时。在较宽的频率和频率范围内研究了制备的Al2O3掺杂的TiO2纳米复合材料的介电性能,交流电导率(sigma(ac)),介电常数(epsilon'),介电损耗(epsilon)和损耗角正切(tanδ)。温度范围。在50Hz和5MHz下测量制备的样品的介电损耗值,发现该值在40℃下在0.11-1.73和在100℃下在0.13-4.39的范围内。还使用高分辨率透射电子显微镜(HRTEM)分析进行了研究。

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