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An alternative process for the preparation of Cu-coated mica composite powder

机译:制备铜包云母复合粉的另一种方法

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Metallization technique based electroless coating is used to prepare Cu-coated mica composite powder. The [Ag(NH3)(2)](+) activator is directly employed to render the surface of mica substrate catalytically active towards copper deposition in the electroless coating solution. The mica powder was characterized by scanning electron microscopy (SEM)/energy-dispersive X-ray (EDX), Auger electron spectroscopy (AES)/X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Fourier transform infra-red spectroscope (FTIR) and transmission electron microscopy (TEM) during and after the coating process. A possible mechanism of electroless copper coating of mica powder utilizing the [Ag (NH3)(2)](+) activator is proposed. The results show that mica powder adsorbs the [Ag(NH3)(2)](+) ions mainly by surface adsorption, and relatively uniform and continuous copper coating, which has fee crystalline structure, is obtained under the giving coating conditions. (c) 2006 Elsevier B.V. All rights reserved.
机译:基于金属化技术的化学镀层用于制备铜包覆的云母复合粉体。 [Ag(NH3)(2)](+)活化剂直接用于使云母基材表面对化学镀液中的铜沉积具有催化活性。云母粉通过扫描电子显微镜(SEM)/能量色散X射线(EDX),俄歇电子能谱(AES)/ X射线光电子能谱(XPS),X射线衍射(XRD),傅里叶变换红外光谱进行表征镀膜过程中和镀膜后的红外光谱仪(FTIR)和透射电子显微镜(TEM)。提出了利用[Ag(NH3)(2)](+)活化剂对云母粉进行化学镀铜的可能机理。结果表明,云母粉主要通过表面吸附来吸附[Ag(NH3)(2)](+)离子,在给定的涂覆条件下获得了较均匀和连续的具有微晶结构的铜涂层。 (c)2006 Elsevier B.V.保留所有权利。

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