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Flavonoids from Geranium robertianum

机译:老鹳草黄酮

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In continuation of research on phenolic compounds from representatives of the Geranium L. genus growing in Georgia, the aerial part (1.0 kg) of G. robertianum L. (Roberts geranium) was treated by the literature method [1]. A yellow solid precipitated from the purified aqueous liquid at room temperature. It was filtered off and recrystallized from pyridine to afford 1. Phenolic compounds were extracted from the mother liquor of 1 by ethylacetate. The total ethylacetate extract was chromatographed over a polyamide column (CH3OH:H2O eluent in various ratios). The enriched total extract and fractions of pure compounds were rechromatographed over a silica-gel:polyamide column to isolate 2-6.
机译:在继续研究佐治亚州生长的天竺葵属的代表的酚类化合物时,用文献方法处理了罗伯特氏天竺葵(罗伯茨天竺葵)的地上部分(1.0千克)[1]。在室温下从纯化的水性液体中沉淀出黄色固体。将其滤出并从吡啶中重结晶,得到1。通过乙酸乙酯从1的母液中提取酚类化合物。将总乙酸乙酯萃取液在聚酰胺柱上进行色谱分离(CH3OH:H2O洗脱液的比例不同)。将富集的总提取物和纯化合物的馏分在硅胶:聚酰胺柱上进行色谱分离,分离出2-6。

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