Synthesis of ethyl 3-cyano-2-methylcinnamates and 3-cyano-2-methylcinnamonitriles from the baylis-hillman acetates

Yun Mi Chung; Ji Hyeon; Jae Nyoung Kim

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Synthesis of ethyl 3-cyano-2-methylcinnamates and 3-cyano-2-methylcinnamonitriles from the baylis-hillman acetates

机译：由Baylis-hillman乙酸酯合成3-氰基-2-甲基肉桂酸乙酯和3-氰基-2-甲基肉桂腈

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The reaction of the DABCO salts 2,generated in situ from the Baylis-Hillman acetates 1,and KCN in aqueous THF gave ehtyl 3-cyano-2-methylcinnamates 4a-d and 3-cyano-2-methylcinnamonitriles 4e-f in good yields.

机译：由Baylis-Hillman乙酸酯1原位生成的DABCO盐2和KCN在THF水溶液中的反应以良好的收率得到3-氰基-2-甲基肉桂酸乙基酯4a-d和3-氰基-2-甲基肉桂腈4e-f。。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2001年第51期|共9页
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Yun Mi Chung; Ji Hyeon; Jae Nyoung Kim;
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正文语种 eng
中图分类有机化学;
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1. Synthesis of ethyl 3-cyano-2-methylcinnamates and 3-cyano-2-methylcinnamonitriles from the baylis-hillman acetates [J] . Yun Mi Chung, Ji Hyeon, Jae Nyoung Kim Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2001,第51期

机译：由Baylis-hillman乙酸酯合成3-氰基-2-甲基肉桂酸乙酯和3-氰基-2-甲基肉桂腈
2. Synthesis of Ethyl 2-Methylene-3-aryl-4-oxoalkanoates and Ethyl 2-Arylidene-4-oxoalkanoates from the Baylis-Hillman Acetates [J] . Jae Nyoung Kim, Jeong Mi Kim, Taek Hyeon Kim, Bulletin of the Korean Chemical Society . 2002,第5期

机译：由Baylis-Hillman乙酸酯合成2-亚甲基-3-芳基-4-氧代链烷酸乙酯和2-亚芳基-4-氧代链烷酸乙酯
3. DABCO catalyzed facile synthesis of highly functionalized pyrazolines from Baylis-Hillman acetates and ethyl diazoacetate [J] . Palakodety Radha Krishna, Y. Lakshmi Prapurna Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2010,第50期

机译：DABCO催化从Baylis-Hillman乙酸盐和重氮乙酸乙酯合成高度官能化的吡唑啉
4. Synthesis of Tannin Phenol Formaldehyde (Tpf) Copolymer from Ethyl Acetate Extract of Green Tea Leaf (Camellia Sinensis) as Bioadhesive Wood [C] . Yusmaniar, Arie Restu, Nurhidayani, International Conference on Industrial, Mechanical, Electrical, and Chemical Engineering . 2019

机译：单宁酚甲醛（TPF）共聚物的合成绿茶叶（Camellia Sinensis）作为生物粘附木材的乙酸乙酯提取物
5. THE SYNTHESIS AND CATALYTIC HYDROGENATION OF SOME KETODIAZOPEPTIDES CATALYTIC HYDROGENATION OF ETHYL PHENOXYACETYLDIAZO ACETATE. [D] . CARPENTER, JAMES WILLIAM. 1965

机译：某些乙二酮乙酸酯的乙二酮双缩合物的催化加氢合成及催化加氢反应。
6. Remarkable rate acceleration of SmI3-mediated iodination of acetates of Baylis-Hillman adducts in ionic liquid: facile synthesis of (Z)-allyl iodides [O] . Yun-Kui Liu, Hui Zheng, Dan-Qian Xu, 2006

机译：离子液体中Baylis-Hillman加合物的乙酸盐的SmI3介导的碘化碘的显着速率加速：（Z）-烯丙基碘化物的简便合成
7. Synthesis of Ethyl 2-Methylene-3-aryl-4-oxoalkanoates and Ethyl 2-Arylidene-4-oxoalkanoates from the Baylis-Hillman Acetates. [O] . Jeong Mi Kim, Yang Jin Im, Taek Hyeon Kim, 2010

机译：合成乙基2-亚甲基-3-芳基-4-氧基烷醇酸盐和乙基2-亚芳基4-氧代苯甲酸盐的合成来自Baylis-Hillman醋酸盐。

Synthesis of ethyl 3-cyano-2-methylcinnamates and 3-cyano-2-methylcinnamonitriles from the baylis-hillman acetates

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