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Studies of the Effect of Surface Modification of Carbon Sorbents by Poly-N-Vinylpyrrolidone Using a Complex of Physicochemical and Microbiological Methods

机译:物理化学和微生物学方法研究聚N-乙烯基吡咯烷酮对碳吸附剂表面改性的影响

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The surface of the VNIITU-1 carbon mesoporous sorbent was modified with poly-N-vinylpyr-rolidone characterized by antibacterial activity. Synthesis was carried out in two stages: (1) impregnation of the carbon sorbent by an aqueous solution of poly-N-vinylpyrrolidone with the molecular mass of 10000 g/mol; and (2) impregnation of the carbon sorbent by an aqueous solution of the (N-vinylpyrrolidone) monomer and initiator with their further polymerization in an inert atmosphere. Carbon sorbent samples were studied using a complex of physicochemical methods: scanning electron microscopy, infrared spectroscopy, low-temperature nitrogen adsorption, nuclear magnetic resonance, and thermogravimetry. It was found that the polymer obtained on the carbon surface is free of the initial toxic VP monomer. Microbiological tests of modified sorbents with respect to pathogenic and opportunistic microflora were carried out.
机译:VNIITU-1碳介孔吸附剂的表面用具有抗菌活性的聚N-乙烯基吡咯烷酮改性。合成分两个阶段进行:(1)用分子量为10000g / mol的聚-N-乙烯基吡咯烷酮的水溶液浸渍碳吸附剂。 (2)在惰性气氛中,用(N-乙烯基吡咯烷酮)单体和引发剂的水溶液浸渍碳吸附剂,并进一步进行聚合。使用多种物理化学方法研究了碳吸附剂样品:扫描电子显微镜,红外光谱,低温氮吸附,核磁共振和热重分析。发现在碳表面上获得的聚合物不含初始有毒VP单体。进行了针对病原菌和机会菌群的改性吸附剂的微生物学测试。

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