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Ultrafine grained bulk ceramic composites consolidated from nanostructured composite powders by pressure less sintering

机译:通过无压烧结从纳米结构复合粉末中固结的超细颗粒大块陶瓷复合材料

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摘要

Nanostructured alumina-titania composite powders which are microsized particles composed of nanosized grains were prepared from nano alumina and titania powders with nanodopants (zirconia and ceria) by ball milling, spray drying and heat treating. Then, the as prepared nanostructured composite powders were consolidated into ultrafine grained alumina-titania bulk ceramic composites through powder compacting and pressure less sintering. The addition of nanodopants leads to a finer grain size in the ceramic and improves the densification of bulk ceramic composite. The active mechanisms of nanodopants were discussed in detail.
机译:通过球磨,喷雾干燥和热处理,由纳米氧化铝和二氧化钛粉末与纳米掺杂剂(氧化锆和二氧化铈)一起制备由纳米晶粒组成的微细颗粒的纳米结构氧化铝-二氧化钛复合粉末。然后,通过粉末压制和无压烧结将所制备的纳米结构复合粉末固结为超细颗粒的氧化铝-二氧化钛块状陶瓷复合材料。纳米掺杂剂的添加导致陶瓷中更细的晶粒尺寸,并改善了块状陶瓷复合材料的致密化。详细讨论了纳米掺杂剂的活性机理。

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