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Wood quality assessment of Pinus radiata (radiata pine) saplings by dynamic mechanical analysis

机译:辐射松树苗的木材力学性能动态力学评估

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摘要

The use of dynamic mechanical analysis was explored as a possible method of screening for wood quality in breeding programmes. Viscoelastic properties along the grain of wood from 18-month-old Pinus radiata saplings were measured using a humidity-controlled dynamic mechanical analyser. Storage modulus and tan delta were determined independently for opposite wood (OW) and compression wood (CW) in 25 trees in the temperature range from 10 to 45 A degrees C at 5 A degrees C intervals at three frequencies (0.1, 1 and 10 Hz) at constant moisture content of 9 %. Storage modulus and tan delta were frequency and temperature dependent. The two wood types did not differ significantly in their storage modulus. But OW exhibited significantly higher tan delta values than CW. The relationship of viscoelastic properties with physical (acoustic velocity, basic density and longitudinal shrinkage) and chemical wood properties was explored. There was a strong correlation (R = 0.76) between storage modulus and dynamic MOE (measured by acoustics). In addition, tan delta was positively correlated with longitudinal shrinkage. Monosaccharide compositions of the cell wall polysaccharides and lignin contents were determined and showed significant differences in the relative proportion of major cell wall components in OW and CW. Correlations between tan delta and xylose, originating from heteroxylans, and lignin content were found for CW, suggesting that the damping behaviour of cell walls is controlled by the matrix between cellulose fibril aggregates.
机译:探索了使用动态力学分析作为育种程序中木材质量筛选的一种可能方法。使用湿度控制的动态机械分析仪,对18个月大的辐射松幼树沿木材的粘弹性进行了测量。在10至45 A摄氏度的温度范围内,以5 A摄氏度的间隔,在三个频率(0.1,1和10 Hz)下,对25棵树中的相对木材(OW)和压缩木材(CW)独立确定储能模量和tanδ。 ),恒定水分含量为9%。储能模量和正切增量取决于频率和温度。两种木材的储能模量没有显着差异。但是OW的tanδ值明显高于CW。探讨了粘弹性与物理(声速,基本密度和纵向收缩率)和化学木材性能之间的关系。储能模量与动态MOE(通过声学测量)之间存在很强的相关性(R = 0.76)。此外,tanδ与纵向收缩呈正相关。测定了细胞壁多糖的单糖组成和木质素含量,并发现OW和CW中主要细胞壁成分的相对比例存在显着差异。发现CW的tanδ和木糖之间的相关性(来自异木聚糖)和木质素含量相关,这表明细胞壁的阻尼行为受纤维素纤维原纤维聚集体之间的基质控制。

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  • 来源
    《Wood Science and Technology》 |2015年第6期|1239-1250|共12页
  • 作者单位

    Univ Canterbury, Sch Forestry, Christchurch 1, New Zealand;

    Univ Auckland, Sch Biol Sci, Auckland 1, New Zealand;

    Inst Wood Sci & Technol, Bangalore 560003, Karnataka, India;

    Univ Manchester, Sch Mat, Ctr Mat Sci, Manchester, Lancs, England;

    Univ Canterbury, Sch Forestry, Christchurch 1, New Zealand;

    Univ Auckland, Sch Biol Sci, Auckland 1, New Zealand;

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